N-羟基邻苯二甲酰亚胺合成路线 (共 297 条)
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane
1 h; Ambient temperature;
参考文献
Kim, Sunggak; Ko, Young Kwan
Journal of the Chemical Society, Chemical Communications, 1985 , # 8 p. 473
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in decane; ethyl acetate
T=20 - 70°C; 12 h;
参考文献
Tan, Bin; Toda, Narihiro; Barbas III, Carlos F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12538 - 12541
Angew. Chem., 2012 , vol. 124, # 50 p. 12706 - 12709,4
反应条件
in tetrahydrofuran
T=20 - 30°C; 12 h;
参考文献
Bailly, Theodorine; Burgada, Ramon
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 63, # 1/2 p. 33 - 43
反应条件
1: acetonitrile / 4 h / 20 °C / |Schlenk technique; |Inert atmosphere
2: [iridium(III)(2-phenylpyridine)3] / acetonitrile / 24 h / 20 °C / |Sealed tube; |Irradiation
View Scheme
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
参考文献
Daicel Chemical Industries, Ltd.
Patent: US6201156 B1, 2001 ;
反应条件
triethylamine in acetone
T=20°C; 2 h;
参考文献
SIRTRIS PHARMACEUTICALS, INC.
Patent: WO2009/146358 A1, 2009 ;
Location in patent: Page/Page column 87 ;
WO 2009/146358 A1
反应条件
triethylamine in acetone
T=20°C; 3 h;
参考文献
SU, Wei-Guo; JIA, Hong; DAI, Guangxiu
Patent: US2012/245178 A1, 2012 ;
Location in patent: Page/Page column 26 ;
US 20120245178 A1
反应条件
triethylamine in acetone
T=4 - 20°C;
参考文献
Tudose, Madalina; Badea, Florin D.; Caproiu, Miron T.; Beteringhe, Adrian; Maganu, Maria; Ionita, Petre; Constantinescu, Titus; Balaban, Alexandru T.
Central European Journal of Chemistry, 2010 , vol. 8, # 4 p. 789 - 796
反应条件
pyridine; toluene
T=80°C;
参考文献
Kuehle; Wegler
Justus Liebigs Annalen der Chemie, 1958 , vol. 616, p. 183,206
反应条件
in cyclohexanone; benzonitrile; cyclohexanol
参考文献
Daicel Chemical Industries, Ltd.
Patent: US6229023 B1, 2001 ;