[2-(联苯-4-基氧基)-乙基]-二甲基-胺合成路线 （共 6 条）
反应条件
potassium carbonate; bis(benzonitrile)palladium(II) dichloride in water; N,N-dimethyl-formamide
T=45°C; 24 h;
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 3765 - 3777
反应条件
potassium carbonate; bis(benzonitrile)palladium(II) dichloride in water; N,N-dimethyl-formamide
T=20°C; Suzuki coupling;
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 3765 - 3777
反应条件
sodium hydroxide in toluene
24 h; Heating;
参考文献
Brown; Cronin; Lan; Nardo
Australian Journal of Chemistry, 1985 , vol. 38, # 5 p. 825 - 833
反应条件
1.1: 82 percent / K2CO3 / ethanol; toluene / 80 °C
2.1: Mg / tetrahydrofuran / 1 h / Heating
2.2: 70 percent / tetrahydrofuran / -78 - 20 °C
3.1: K2CO3 / PdCl2(PhCN)2 / dimethylformamide; H2O / 20 °C
View Scheme
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 3765 - 3777
反应条件
1.1: Mg / tetrahydrofuran / 1 h / Heating
1.2: 70 percent / tetrahydrofuran / -78 - 20 °C
2.1: K2CO3 / PdCl2(PhCN)2 / dimethylformamide; H2O / 20 °C
View Scheme
参考文献
Zhou, Chengxiang; Larock, Richard C.
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 3765 - 3777
参考文献
Strickler,H.
Diss. <Univ. Paris 1938> S. 26
