2,2-(乙烯二硫代)二苯胺合成路线 （共 11 条）
反应条件
in N-methyl-acetamide
参考文献
The United States of America as Represented by the United States Department of Energy
Patent: US4564683 A1, 1986 ;
反应条件
potassium fluoride on basic alumina; [Bmim][Br] T=85°C; 3 h;
参考文献
Chhikara, Bhupender S.; Mishra, Anil K.; Tandon, Vibha
Heterocycles, 2004 , vol. 63, # 5 p. 1057 - 1065
反应条件
Yield given. Multistep reaction;
参考文献
Sellmann, Dieter; Boehlen, Elmar
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1982 , vol. 37, # 8 p. 1026 - 1033
反应条件
sodium ethanolate in ethanol
0.5 h; Heating;
参考文献
Kumar; Sharma nee Bhalla; Sharma
Journal of Chemical Research - Part S, 2000 , # 10 p. 492 - 493
反应条件
1: 2-amino-benzenethiol With potassium hydroxide in isopropyl alcohol
Inert atmosphere;
2: 1,2-di-iodoethane in isopropyl alcohol
T=50 - 80°C; 9.15 h;
参考文献
PRC DeSoto International, Inc.; Hobbs, Stephen J.; Ito, Marfi; Cai, Juexiao; Rao, Chandra; Lin, Renhe
Patent: US2013/71571 A1, 2013 ;
Location in patent: Paragraph 0846 ;
反应条件
hydrazine hydrate; palladium on activated charcoal in ethanol
7 h; Heating;
参考文献
Das, Sanjib; Nag, Amit; Sadhu, Kalyan K.; Goswami, Debabrata; Bharadwaj, Parimal K.
Journal of Organometallic Chemistry, 2007 , vol. 692, # 22 p. 4969 - 4977
反应条件
1: alkali
2: tin; hydrochloric acid
View Scheme
参考文献
Fromm; Benzinger; Schaefer
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 331
反应条件
1: cyclobenzothiazole With sodium hydroxide in water
Reflux;
2: 1,2-dichloro-ethane T=60 - 65°C; 2 h; Reagent/catalystTemperature;
参考文献
Densmore, Crystal G.; Wheeler, Hilary; Cohenour, Rebecca; Robison, Thomas W.; Hasam, Dawud; Cordova, Blossom J.; Stark, Peter C.; Fuller, Edward N.; Cook, Charles J.; Weber, Holly A.
Organic Process Research and Development, 2007 , vol. 11, # 6 p. 996 - 1003
反应条件
1: cyclobenzothiazole With sodium hydroxide in water
T=116°C; 4 h;
2: ethylene dibromide T=105°C; 2.33333 h;
参考文献
Densmore, Crystal G.; Wheeler, Hilary; Cohenour, Rebecca; Robison, Thomas W.; Hasam, Dawud; Cordova, Blossom J.; Stark, Peter C.; Fuller, Edward N.; Cook, Charles J.; Weber, Holly A.
Organic Process Research and Development, 2007 , vol. 11, # 6 p. 996 - 1003
反应条件
in methanol
10 h; Heating;
参考文献
Shukla, P R; Pathak, Ashish K; Ahmad, Nihal
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1992 , vol. 31, # 3 p. 205 - 209
