4-碘-2-甲基-1-硝基苯合成路线 （共 12 条）
反应条件
1.1: GNO3 / sulfuric acid / 1 h / 0 - 5 °C
2.1: sulfuric acid; sodium nitrite / water / 0.17 h / 0 °C
2.2: 3.67 h / 0 - 20 °C
View Scheme
参考文献
Bao, Chunyan; Jin, Ming; Li, Bo; Xu, Yaodong; Jin, Jingyan; Zhu, Linyong
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 27 p. 5238 - 5244
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
1.) THF, -70 deg C, 10 min, 2.) 3 h, 0 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bartoli, G.; Bosco, M.; Dalpozzo, R.
Tetrahedron Letters, 1985 , vol. 26, # 1 p. 115 - 118
