DL-N-苯甲酰-2-苄基丝氨酸合成路线 （共 4 条）
反应条件
2: 76.5 percent / pyridine / 72 h / 0 °C 3: 69.2 percent / NaI, Zn / dimethylformamide / 10 h / 120 °C 4: 4 N HCl / 5 h / Heating View Scheme
参考文献
Olma
Polish Journal of Chemistry, 1996 , vol. 70, # 11 p. 1442 - 1447
反应条件
sodium hydroxide in 1,4-dioxane
1 h;
参考文献
Olma
Polish Journal of Chemistry, 1996 , vol. 70, # 11 p. 1442 - 1447
反应条件
1: 121 g / pyridine / H2O / 12 h / 20 °C
2: 89.2 percent / aq. NaOH / dioxane / 1 h / 20 °C
View Scheme
参考文献
Shiraiwa, Tadashi; Suzuki, Masahiro; Sakai, Yoshio; Nagasawa, Hisashi; Takatani, Kazuhiro; Noshi, Daisuke; Yamanashi, Kenji
Chemical and pharmaceutical bulletin, 2002 , vol. 50, # 10 p. 1362 - 1366
反应条件
1: Ac2O / 1 h / 95 °C
2: 121 g / pyridine / H2O / 12 h / 20 °C
3: 89.2 percent / aq. NaOH / dioxane / 1 h / 20 °C
View Scheme
参考文献
Shiraiwa, Tadashi; Suzuki, Masahiro; Sakai, Yoshio; Nagasawa, Hisashi; Takatani, Kazuhiro; Noshi, Daisuke; Yamanashi, Kenji
Chemical and pharmaceutical bulletin, 2002 , vol. 50, # 10 p. 1362 - 1366
