N-[(E)-(二甲基氨基)亚甲基]硫代苯甲酰胺合成路线 （共 10 条）
反应条件
ammonium chloride 1.) -70 deg C, 30 min, THF; 2.) r.t., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 12, p. 325 - 340
反应条件
T=900°C; P=0.003 Torr; 0.75 h; Mechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 589 - 595
反应条件
ammonium chloride 1.) -70 deg C, 30 min, THF; 2.) r.t., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 12, p. 325 - 340
反应条件
ammonium chloride 1.) -70 deg C, 30 min, THF; 2.) r.t., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Guemas, Jean-Pierre; Lees, Michele; Reliquet, Alain; Villieras, Jean
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 12, p. 325 - 340
反应条件
ammonium chloride 1.) -70 deg C, 30 min, THF; 2.) r.t., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Guemas, Jean-Pierre; Lees, Michele; Reliquet, Alain; Villieras, Jean
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 12, p. 325 - 340
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; ammonium chloride 1.) THF, -50 deg C, 4 h; 2.) water, -80 deg C; Yield given. Multistep reaction;
参考文献
Guemas, Jean-Pierre; Villieras, Jean
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 26, p. 299 - 306
反应条件
hydroquinone in dichloromethane
2 h; Ambient temperature;
参考文献
Pradere, J. P.; Roze, J. C.; Quiniou, H.; Danion-Bougot, R.; Danion, D.; Toupet, L.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 597 - 602
反应条件
in benzene
T=140°C; 5 h; other N'-(thioacyl)formamidines; var. solvents, var. times and temp.; Product distribution;
参考文献
Gokou, Celestin Tea; Pradere, Jean-Paul; Quiniou, Herve
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1545 - 1547
反应条件
1: 98 percent / benzene / 5 h / 140 °C
2: 98 percent / benzene / 5 h / 140 °C
View Scheme
参考文献
Gokou, Celestin Tea; Pradere, Jean-Paul; Quiniou, Herve
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1545 - 1547
参考文献
Meslin,J.C.; Quiniou,H.
Tetrahedron, 1975 , vol. 31, p. 3055 - 3058
