3,6-二硫杂-1,8-辛二醇合成路线 （共 42 条）
反应条件
quinoline in ethanol
参考文献
Hoffmann-La Roche Inc.
Patent: US4345084 A1, 1982 ;
反应条件
sodium periodate in methanol
T=20°C; 1 h;
参考文献
Timperley, Christopher M.; Black, Robin M.; Bird, Michael; Holden, Ian; Mundy, Joanna L.; Read, Robert W.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 9 p. 2027 - 2046
参考文献
American Cyanamid Company
Patent: US4762935 A1, 1988 ;
反应条件
1: diethyl ether; SOCl2 / zuletzt bei Siedetemperatur
2: Na2CO3; ethanol
View Scheme
参考文献
Price; Roberts
Journal of Organic Chemistry, 1947 , vol. 12, p. 264,266
参考文献
Hoffmann-La Roche Inc.
Patent: US3978093 A1, 1976 ;
反应条件
in hydrogenchloride
PdCl2 was dissolved with heating in H2O and 36percent HCl added; addn. of an aq. soln. of C6H14S2O2;; evapn. to dryness at 40°C; dried in vac. over P2O5 for 72 h; treated with CHCl3; crystn. after 2 weeks; filtration; dried; recrystn. from acetone; elem. anal.;;
参考文献
Zhuravleva, M. A.; Pavlishchuk, V. V.; Kurbakova, A. P.; Efimenko, I. A.; Yatsimirskii, K. B.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1991 , vol. 36, p. 982 - 985
Zhurnal Neorganicheskoi Khimii, 1991 , vol. 36, p. 1737 - 1742
反应条件
in water
addn. of an aq. soln. of C6H14S2O2 to an aq. soln. of K2PdCl4 (molar ratio = 1:1);; evapn. to dryness at 40°C; dried in vac. over P2O3 for 72 h; treated with a large amt. of acetone; evapn. to dryness; addn. of CHCl3; crystn. after two weeks; filtration; washed with CHCl3; dried in vac.; elem. anal.;;
参考文献
Zhuravleva, M. A.; Pavlishchuk, V. V.; Kurbakova, A. P.; Efimenko, I. A.; Yatsimirskii, K. B.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1991 , vol. 36, p. 982 - 985
Zhurnal Neorganicheskoi Khimii, 1991 , vol. 36, p. 1737 - 1742
反应条件
in benzene
stirring (room temp., overnight); filtration; elem. anal.;
参考文献
Kaminskaia, Natalia V.; Guzei, Ilia A.; Kostic, Nenad M.
Journal of the Chemical Society - Dalton Transactions, 1998 , # 22 p. 3879 - 3885
反应条件
in methanol; dichloromethane; ethyl acetate
参考文献
Hoffmann-La Roche Inc.
Patent: US4544770 A1, 1985 ;
反应条件
1: diethyl ether; SOCl2 / zuletzt bei Siedetemperatur
2: H2O2; glacial acetic acid
3: dioxane
View Scheme
参考文献
Price; Roberts
Journal of Organic Chemistry, 1947 , vol. 12, p. 264,266
