in neat (no solvent) irreversible cleveage of (C2H5)2S on heating in vac.;;
参考文献
Fergusson, J. E.; Karran, J. D.; Seevaratnam, S.
Journal of the Chemical Society, 1965 , p. 2627 - 2630
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Gmelin Handbook: Ru: SVol., 173, page 469 - 471
mercury; zinc in tetrahydrofuran addn. of Zn-amalgam to a soln. of (RuCl3(S(C2H5)2)3) in dry THF; stirring for 90 minutes; addn. of NaC5H5; stirring at room temp. for 16 h; performed under N2;; filtration through Celite; evapn.; chromy. (silica gel, CCl4); evapn.;;
参考文献
Haas, T. J.; Mueller-Westerhoff, U. T.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1992 , vol. 22, p. 227 - 246
