您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-溴吲哚
合成路线
（共 87 条）
90481-67-7
→
反应条件
52488-36-5
4-溴吲哚
反应条件
1: 85.1 percent / Et3N / CH2Cl2 / 1 h / Ambient temperature 2: 96.6 percent / Fe / acetic acid; ethanol / 5 h / Heating 3: 46.3 percent / p-benzoquinone, LiCl, PdCl2(CH3CN)2 / tetrahydrofuran / 22 h / 100 °C / sealed tube View Scheme
参考文献
Harrington, Peter J.; Hegedus, Louis S.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2658 - 2662
1280538-41-1
→
反应条件
52488-36-5
4-溴吲哚
反应条件
iron; acetic acid in ethanol T=50°C; 0.5 h; RefluxInert atmosphere;
参考文献
Griffiths-Jones, Charlotte M.; Knight, David W.
Tetrahedron, 2011 , vol. 67, # 44 p. 8515 - 8528
85355-50-6
→
反应条件
52488-36-5
4-溴吲哚
反应条件
sodium acetate; iron; acetic acid in ethanol; water 2 h; Heating; Yield given;
参考文献
Raucher, Stanley; Koolpe, Gary A.
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2066 - 2069
85355-40-4
→
反应条件
52488-36-5
4-溴吲哚
反应条件
sodium acetate; iron; acetic acid in ethanol; water 2 h; Heating;
参考文献
Raucher, Stanley; Koolpe, Gary A.
Journal of Organic Chemistry, 1983 , vol. 48, # 12 p. 2066 - 2069
90481-71-3
→
反应条件
52488-36-5
4-溴吲哚
反应条件
1: 76.7 percent / p-benzoquinone, LiCl, PdCl2(CH3CN)2 / tetrahydrofuran / 18 h / Heating 2: 98 percent / 20percent aq. NaOH / methanol / 12 h / Heating View Scheme
参考文献
Harrington, Peter J.; Hegedus, Louis S.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2658 - 2662
16732-64-2
4-溴吲哚-2-羧酸
→
反应条件
52488-36-5
4-溴吲哚
反应条件
quinoline; copper(I) bromide T=250°C;
参考文献
Pappalardo; Vitali
Gazzetta Chimica Italiana, 1958 , vol. 88, p. 1147,1153, 1159
Full Text Show Details
Plieninger
Chemische Berichte, 1955 , vol. 88, p. 370,373
863870-72-8
二乙基氨基甲酸(3-溴苯基)酯
→
反应条件
52488-36-5
4-溴吲哚
反应条件
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C 2.1: sodium hydroxide / ethanol / Reflux 3.1: sodium hydroxide / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere 3.2: 2 h / 20 °C / Inert atmosphere 4.1: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere 5.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / N,N-dimethyl-formamide / 3 h / 40 °C / Inert atmosphere 6.1: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 140 °C / Inert atmosphere View Scheme
参考文献
Guilarte, Veronica; Castroviejo, M. Pilar; Garcia-Garcia, Patricia; Fernandez-Rodriguez, Manuel A.; Sanz, Roberto
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3416 - 3437
863870-79-5
N,N-二乙基-氨基甲酸 3-溴-2-碘苯基酯
→
反应条件
52488-36-5
4-溴吲哚
反应条件
1.1: sodium hydroxide / ethanol / Reflux 2.1: sodium hydroxide / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere 3.1: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere 4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / N,N-dimethyl-formamide / 3 h / 40 °C / Inert atmosphere 5.1: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 140 °C / Inert atmosphere View Scheme
参考文献
Guilarte, Veronica; Castroviejo, M. Pilar; Garcia-Garcia, Patricia; Fernandez-Rodriguez, Manuel A.; Sanz, Roberto
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3416 - 3437
1244651-37-3
→
反应条件
52488-36-5
4-溴吲哚
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / N,N-dimethyl-formamide / 3 h / 40 °C / Inert atmosphere 2: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 140 °C / Inert atmosphere View Scheme
参考文献
Guilarte, Veronica; Castroviejo, M. Pilar; Garcia-Garcia, Patricia; Fernandez-Rodriguez, Manuel A.; Sanz, Roberto
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3416 - 3437
1287791-68-7
→
反应条件
52488-36-5
4-溴吲哚
反应条件
1: sodium hydroxide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere 2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diethylamine / N,N-dimethyl-formamide / 3 h / 40 °C / Inert atmosphere 3: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 140 °C / Inert atmosphere View Scheme
参考文献
Guilarte, Veronica; Castroviejo, M. Pilar; Garcia-Garcia, Patricia; Fernandez-Rodriguez, Manuel A.; Sanz, Roberto
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3416 - 3437
首页
上一页
1
2
3
4
5
6
...
9
下一页
末页
到第
页
确定
