三(二亚苄基丙酮)二钯-氯仿加合物合成路线 (共 6 条)
参考文献
Gushchin; Grunova; Moiseev; Morozov; Shavyrin; Dodonov
Russian Chemical Bulletin, 2003 , vol. 52, # 6 p. 1376 - 1379
反应条件
in benzene stirred at room temp. under Ar for 1 wk;
参考文献
Nakano, Taichi; Ono, Kazuyoshi; Senda, Yoshiya; Migita, Toshihiko
Journal of Organometallic Chemistry, 2001 , vol. 619, # 1-2 p. 313 - 317
反应条件
Product distribution / selectivity;
参考文献
Universitetet i Olso
Patent: US2007/203159 A1, 2007 ;
Location in patent: Page/Page column 8; 22 ;
反应条件
1,2-bis-(diphenylphosphino)ethane in benzene addn. of bis(diphenylphosphino)ethane to a stirred soln. of Pd2(CO(CHCHC6H5)2)3CHCl3 in degassed benzene under dry N2; stirring for 1 h;; removal of solvent in vac.; treatment with ice-cold degassed acetone; filtration; washed with cold acetone; drying;;
参考文献
Journal of the American Chemical Society, , vol. 114, # 17 p. 6858 - 6863
反应条件
in dichloromethane (N2), Pd complex in CH2Cl2 added to PPh3 in CH2Cl2, stirred for 0.2 h, treated with ligand in CH2Cl2, stirred for 0.2 h; concd.(vac.), pptd.(petroleum ether), filtered, washed (hexane), recrystd., elem. anal.;
参考文献
Crawforth, Catherine M.; Burling, Suzanne; Fairlamb, Ian J. S.; Taylor, Richard J. K.; Whitwood, Adrian C.
Chemical Communications, 2003 , # 17 p. 2194 - 2195
反应条件
in water; ethyl acetate; toluene
参考文献
Cambridge Display Technology Limited; Sumitomo Chemical Co., Ltd; Kamtekar, Kiran; Steudel, Annette
Patent: EP2738195 A1, 2014 ;
Location in patent: Page/Page column ;