N-(对甲苯)氨基甲酸乙酯合成路线 （共 32 条）
反应条件
phosphorus pentoxide
参考文献
Hofmann,A. W.
Chemische Berichte, 1870 , vol. 3, p. 655
反应条件
1: With trifluoroacetic acid
1 h; Heating;
2: With potassium hydroxide; potassium hexacyanoferrate(III) in ethanol; water
4 h; Heating;
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Barbieri, Vera; Pastorini, Giovanni; Manzini, Paolo; Guiotto, Adriano
Tetrahedron, 2006 , vol. 62, # 52 p. 12351 - 12356
反应条件
1: 98 percent / TFA / 0.17 h / 110 °C / microwave irradiation
2: 97 percent / K3Fe(CN)6; KOH / H2O; ethanol / 0.67 h / 100 °C / microwave irradiation
View Scheme
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Barbieri, Vera; Pastorini, Giovanni; Manzini, Paolo; Guiotto, Adriano
Tetrahedron, 2006 , vol. 62, # 52 p. 12351 - 12356
反应条件
trifluoroacetic acid
T=110°C; 0.166667 h; microwave irradiation;
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Guiotto, Adriano
Tetrahedron Letters, 2007 , vol. 48, # 18 p. 3229 - 3231
反应条件
1: 80 percent / trifluoroacetic acid / 1 h / Heating
2: 92 percent / potassium hydroxide / H2O / 2 h / Heating
View Scheme
参考文献
Chilin, Adriana; Marzaro, Giovanni; Zanatta, Samuele; Barbieri, Vera; Pastorini, Giovanni; Manzini, Paolo; Guiotto, Adriano
Tetrahedron, 2006 , vol. 62, # 52 p. 12351 - 12356
参考文献
Dixon
Journal of the Chemical Society, 1901 , vol. 79, p. 104
反应条件
T=230 - 240°C; 0.5 h;
参考文献
Hassan, Alaa A; Mourad, Aboul-fetouh E
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 4 p. 277 - 279
Title/Abstract Full Text Show Details
Hassan, Alaa A.; Mourad, Aboul-Fetouh E.
Revue Roumaine de Chimie, 1994 , vol. 39, # 4 p. 397 - 404
反应条件
hydrazine hydrate
24 h; Reflux;
参考文献
Aboul-Enein, Mohamed N.; El-Azzouny, Aida A.; Attia, Mohamed I.; Maklad, Yousreya A.; Amin, Kamilia M.; Abdel-Rehim, Mohamed; El-Behairy, Mohammed F.
European Journal of Medicinal Chemistry, 2012 , vol. 47, # 1 p. 360 - 369
反应条件
1: 25 percent Spectr. / 97 - 99percent H2SO4 / 3 h / 50 °C
2: 30 percent / 90percent H2SO4 / 3 h / 100 °C
View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1990 , vol. 43, # 2 p. 339 - 353
反应条件
(i) Na, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Jancke,H. et al.
Journal of Organometallic Chemistry, 1977 , vol. 134, p. 21 - 29
