3-甲基-1H-吲哚-2-甲醛合成路线 （共 33 条）
反应条件
1: NBS; benzoyl peroxide / CCl4 / Heating 2: 25 percent / 2-nitropropane; NaOEt / ethanol / 10 h / 20 °C View Scheme
参考文献
Mohanakrishnan, Arasambattu K.; Balamurugan, Ramalingam; Ramesh, Neelamegam
Tetrahedron Letters, 2005 , vol. 46, # 47 p. 8189 - 8193
反应条件
1: n-BuLi / tetrahydrofuran; hexane / 0.08 h / 25 °C 2: t-BuLi / tetrahydrofuran; pentane / 3 h / -70 °C 3: 54 percent / Heating View Scheme
参考文献
Katritzky, Alan R.; Akutagawa, Kunihiko; Jones, R Alan
Synthetic Communications, 1988 , vol. 18, # 10 p. 1151 - 1158
反应条件
1: 56 percent / benzene / 20 h / 60 °C 2: t-butylhypochlorite / tetrahydrofuran 3: 80 percent / Et3N / tetrahydrofuran 4: H2O View Scheme
参考文献
Wilson, R. Marshall; Hengge, Alvan
Tetrahedron Letters, 1985 , vol. 26, # 31 p. 3673 - 3676
反应条件
1: 80 percent / Et3N / tetrahydrofuran 2: H2O View Scheme
参考文献
Wilson, R. Marshall; Hengge, Alvan
Tetrahedron Letters, 1985 , vol. 26, # 31 p. 3673 - 3676
反应条件
potassium hydroxide 0.75 h; Heating;
参考文献
Benzies, David W.M.; Fresneda, Pilar Martinez; Jones, R. Alan
Synthetic Communications, 1986 , vol. 16, # 14 p. 1799 - 1808
反应条件
sodium 0.75 h; Heating;
参考文献
Benzies, David W.M.; Fresneda, Pilar Martinez; Jones, R. Alan
Synthetic Communications, 1986 , vol. 16, # 14 p. 1799 - 1808
反应条件
1: 85 percent / AcOH / 3 h / 80 °C 2: 33 percent / selenium oxide / dioxane; H2O / 4 h / 50 °C View Scheme
参考文献
Rodriguez; Lafuente; Garcia-Almaraz
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 5 p. 1281 - 1288
反应条件
acid-washed montmorillonite K10 clay (acid-clay) T=20°C; 4 h;
参考文献
Chakrabarty, Manas; Mukherji, Ajanta
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1681 - 1694
反应条件
1: pyridine / dichloromethane / 3.25 h / 0 - 20 °C / |Inert atmosphere 2: tetrahydrofuran / 3 h / |Reflux 3: N-iodo-succinimide / water; acetone / 24 h / |Reflux View Scheme
参考文献
Kothandaraman, Prasath; Lauw, Sherman Jun Liang; Chan, Philip Wai Hong
Tetrahedron, 2013 , vol. 69, # 35 p. 7471 - 7480
反应条件
1: tetrahydrofuran / 3 h / |Reflux 2: N-iodo-succinimide / water; acetone / 24 h / |Reflux View Scheme
参考文献
Kothandaraman, Prasath; Lauw, Sherman Jun Liang; Chan, Philip Wai Hong
Tetrahedron, 2013 , vol. 69, # 35 p. 7471 - 7480
