6-甲基-3-环己烯-1-甲醇合成路线 （共 5 条）
反应条件
iron(III) tosylate hexahydrate in methanol T=20°C; 3 h; chemoselective reaction;
参考文献
Bothwell, Jason M.; Angeles, Veronica V.; Carolan, James P.; Olson, Margaret E.; Mohan, Ram S.
Tetrahedron Letters, 2010 , vol. 51, # 7 p. 1056 - 1058
参考文献
French; Gallagher
Journal of the American Chemical Society, 1942 , vol. 64, p. 1497
反应条件
lithium aluminium tetrahydride
参考文献
Knight, David W.; Ojhara, Bol
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 5 p. 955 - 960
反应条件
1: (i) MeSO2Cl, Py, (ii) LiAlH4, Et2O
2: (i) B2H6, (ii) CrO3, H2SO4
View Scheme
参考文献
Tichy,M. et al.
Collection of Czechoslovak Chemical Communications, 1970 , vol. 35, p. 1522 - 1535
反应条件
1: 97 g / pyridine / 16 h / 0 °C
2: 13 g / LiAlH4 / 1.) THF, ice-cold, 48 h, 2.) reflux, 1 h
View Scheme
参考文献
Knight, David W.; Ojhara, Bol
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 5 p. 955 - 960
