1,3-氧氮杂己环-2-酮合成路线 (共 30 条)
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C;
参考文献
MERCK and CO., INC.
Patent: WO2009/123870 A1, 2009 ;
Location in patent: Page/Page column 62 ;
WO 2009/123870 A1
反应条件
1: in tetrahydrofuran T=-5 - 20°C; 2.5 h; 2: With cesium fluoride in tetrahydrofuran
参考文献
International Business Machines Corporation
Patent: US2010/280242 A1, 2010 ;
Location in patent: Page/Page column 6 ;
反应条件
nanoparticulated CeO2 in ethanol T=160°C; P=5250.53 Torr; 6 h; Sealed reactor;
参考文献
Juarez, Raquel; Concepcion, Patricia; Corma, Avelino; Garcia, Hermenegildo
Chemical Communications, 2010 , vol. 46, # 23 p. 4181 - 4183
反应条件
bis-triphenylphosphine-palladium(II) chloride; oxygen; triethylamine hydroiodide; triethylamine in acetonitrile T=59.84°C; P=750.075 Torr; 7 h;
参考文献
Giannoccaro, Potenzo; Ferragina, Carla; Gargano, Michele; Quaranta, Eugenio
Applied Catalysis A: General, 2010 , vol. 375, # 1 p. 78 - 84
反应条件
in 1,3,5-trimethyl-benzene T=160°C;
参考文献
Masuyama, Araki; Tsuchiya, Kikuo; Okahara, Mitsuo
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 10 p. 2855 - 2859
反应条件
zinc oxide in N,N-dimethyl-formamide T=120°C; P=532.553 Torr; 0.166667 h; microwave irradiation;
参考文献
Kim, Yong Jin; Varma, Rajender S.
Tetrahedron Letters, 2004 , vol. 45, # 39 p. 7205 - 7208
反应条件
triethylamine in dichloromethane
参考文献
Poindexter; Strauss
Synthetic Communications, 1993 , vol. 23, # 9 p. 1329 - 1338
参考文献
Hall; Schneider
Journal of the American Chemical Society, 1958 , vol. 80, p. 6409,6412
参考文献
Korepin; Galkin; Glushakova; Perepelkina; Loginova; Lodygina; Ol'khov; Eremenko
Russian Chemical Bulletin, 2003 , vol. 52, # 10 p. 2221 - 2230
参考文献
Willer, Rodney L.; Campbell, Christopher G.; Storey, Robson F.
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 2 p. 421 - 423