1,3-氧氮杂己环-2-酮合成路线 (共 30 条)
反应条件
tetrachloromethane; triethylamine; triphenylphosphine in acetonitrile P=760 Torr; 20 h; Ambient temperature;
参考文献
Kubota, Yasuhiko; Kodaka, Masato; Tomohiro, Takenori; Okuno, Hiroaki (Yohmei)
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 1 p. 5 - 6
反应条件
in acetonitrile Ambient temperature;
参考文献
Inesi; Mucciante; Rossi
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 1337 - 1338
反应条件
N-ethyl-N,N-diisopropylamine in chloroform Heating;
参考文献
Curran, Timothy P.; Pollastri, Michael P.; Abelleira, Susan M.; Messier, Renee J.; McCollum, Theresa A.; Rowe, Campbell G.
Tetrahedron Letters, 1994 , vol. 35, # 30 p. 5409 - 5412
反应条件
in methanol T=60°C; 24 h;
参考文献
Leung, Man-Kit; Lai, Jun-Liang; Lau, King-Hang; Yu, Hsiao-Hua; Hsiao, Hsiang-Ju
Journal of Organic Chemistry, 1996 , vol. 61, # 12 p. 4175 - 4179
反应条件
T=180°C; P=75007.5 Torr; 24 h; Autoclave;
参考文献
Wu, Chaoyong; Cheng, Haiyang; Liu, Ruixia; Wang, Qiang; Hao, Yufen; Yu, Yancun; Zhao, Fengyu
Green Chemistry, 2010 , vol. 12, # 10 p. 1811 - 1816
参考文献
Delaby et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1954 , vol. 239, p. 674
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Najer et al.
Bulletin de la Societe Chimique de France, 1959 , p. 1611,1614
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Dyer; Scott
Journal of the American Chemical Society, 1957 , vol. 79, p. 672,674
反应条件
oxygen; N(Et)4ClO4 1.) -1.0 V vs SCE, MeCN, 2.) room temperature, overnight; Yield given. Multistep reaction;
参考文献
Casadei, Maria Antonietta; Moracci, Franco Micheletti; Zappia, Giovanni; Inesi, Achille; Rossi, Leucio
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6754 - 6759
参考文献
Delaby; Damiens
Festschr. Stoll <Basel 1957> S. 474
反应条件
anschliessend Erhitzen mit K2CO3 auf 160grad;
参考文献
Dyer; Read
Journal of Organic Chemistry, 1959 , vol. 24, p. 1788
参考文献
Dyer; Read
Journal of Organic Chemistry, 1959 , vol. 24, p. 1788
Full Text View citing articles Show Details
Delaby et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1954 , vol. 239, p. 674