7-甲氧基-1,3-苯并二氧化物-5-羧酸合成路线 （共 21 条）
反应条件
1: With ammonium hydroxide; iodine in tetrahydrofuran; water
T=20°C; 16 h;
2: With potassium permanganate in tetrahydrofuran; water; acetone
4 h; Reflux;
参考文献
Semenov, Victor V.; Kiselyov, Alex S.; Titov, Ilia Y.; Sagamanova, Irina K.; Ikizalp, Natalie N.; Chernysheva, Natalia B.; Tsyganov, Dmitry V.; Konyushkin, Leonid D.; Firgang, Sergei I.; Semenov, Roman V.; Karmanova, Irina B.; Raihstat, Mikhail M.; Semenova, Marina N.
Journal of Natural Products, 2010 , vol. 73, # 11 p. 1796 - 1802
反应条件
potassium permanganate; water
参考文献
Mitsuhashi et al.
Yakugaku Zasshi, 1959 , vol. 79, p. 106
Chem.Abstr., 1959 , p. 10104
反应条件
1.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C
2.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C
2.2: 4 h / Reflux
View Scheme
参考文献
Semenov, Victor V.; Kiselyov, Alex S.; Titov, Ilia Y.; Sagamanova, Irina K.; Ikizalp, Natalie N.; Chernysheva, Natalia B.; Tsyganov, Dmitry V.; Konyushkin, Leonid D.; Firgang, Sergei I.; Semenov, Roman V.; Karmanova, Irina B.; Raihstat, Mikhail M.; Semenova, Marina N.
Journal of Natural Products, 2010 , vol. 73, # 11 p. 1796 - 1802
反应条件
potassium hydroxide in methanol
9 h; Heating;
参考文献
Vyas, Ashok V.; Mulchandani, Mewand B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 12 p. 2945 - 2947
反应条件
potassium permanganate; water in acetone
4 h; Reflux;
参考文献
Konyushkin; Godovikova; Vorontsova; Tsyganov; Karmanova; Raihstat; Firgang; Pokrovskii; Semenova; Semenov
Russian Chemical Bulletin, 2010 , vol. 59, # 12 p. 2268 - 2275
反应条件
potassium hydroxide in ethanol
24 h; Heating;
参考文献
Chen; Hsu
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 166 - 169
反应条件
potassium hydroxide in ethanol
24 h; Heating;
参考文献
Chen; Hsu
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 166 - 169
反应条件
potassium permanganate; ethanol; sodium sulfate
Reagens 4: Magnesiumcarbonat;
参考文献
Kindler; Peschke
Archiv der Pharmazie (Weinheim, Germany), 1932 , vol. 270, p. 353,359
反应条件
potassium permanganate; water
参考文献
Rao; Seshadri
Proceedings - Indian Academy of Sciences, Section A, 1946 , # 23 p. 147,150
反应条件
ethanol; sulfuric acid
Erwaermen des Reaktionsprodukts mit Dijodmethan, Kaliumcarbonat und Aceton und Erhitzen des Reaktionsprodukts mit aethanol. Kalilauge;
参考文献
Seshadri; Thiruvengadam
Proceedings - Indian Academy of Sciences, Section A, 1950 , # 32 p. 27
