反应条件
1: 55.3 g / AnalaR pyridine / 1 h / Ambient temperature
2: 58.2 g / sodium hydride / tetrahydrofuran / 1.) reflux, 5 min, 2.) room temperature, 0.5 h
3: 38.0 g / KOH, H2O / methanol / 1 h
4: 1.) methanesulphonyl chloride, 2.) sodium iodide / 1.) pyridine, 0.5 h, room temperature, 2.) acetone, 0.5 h, reflux
View Scheme
参考文献
Leeson, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2125 - 2128
