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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
52631-78-4
合成路线
（共 12 条）
52631-78-4
→
反应条件
75883-39-5
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 37 percent / aq. NaOH / 2 h / 90 °C 3: 52 percent / KI / acetonitrile / 24 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
75883-55-5
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 37 percent / aq. NaOH / 2 h / 90 °C 3: 30 percent / KI / acetonitrile / 24 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
75883-62-4
1-[4,7-二甲氧基-6-(4-哌啶-1-基丁氧基)-1-苯并呋喃-5-基]-3-甲基脲
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 71 percent / K2CO3 / acetonitrile / 6 h / Heating 3: 40 percent / KI / acetonitrile / 24 h / Heating 4: 70 percent / 2 N HCl / 5 h / Heating 5: 79 percent / toluene / 5 h / Ambient temperature View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
75902-75-9
1-[6-[2-(二丙基氨基)乙氧基]-4,7-二甲氧基-1-苯并呋喃-5-基]-3-甲基脲
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 90 percent / HCl / ethanol / 20 h / Heating 3: 89 percent / CHCl3 / 2 h / Ambient temperature 4: 77 percent / K2CO3 / acetonitrile / 4 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
66202-98-0
1-(4,7-二甲氧基-6-(2-(二甲基氨基)乙氧基)-5-苯并呋喃基)-3-甲基-脲
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 90 percent / HCl / ethanol / 20 h / Heating 3: 89 percent / CHCl3 / 2 h / Ambient temperature 4: 53 percent / K2CO3 / acetonitrile / 4 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
66202-99-1
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 90 percent / HCl / ethanol / 20 h / Heating 3: 89 percent / CHCl3 / 2 h / Ambient temperature 4: 58 percent / K2CO3 / acetonitrile / 4 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
66203-00-7
卡罗卡尼
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 90 percent / HCl / ethanol / 20 h / Heating 3: 89 percent / CHCl3 / 2 h / Ambient temperature 4: 37 percent / K2CO3 / acetonitrile / 4 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
66203-02-9
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 90 percent / HCl / ethanol / 20 h / Heating 3: 89 percent / CHCl3 / 2 h / Ambient temperature 4: 62 percent / K2CO3 / acetonitrile / 4.5 h / Heating 5: 64 percent / NaI, K2CO3 / acetonitrile / 15 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
66203-04-1
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 90 percent / HCl / ethanol / 20 h / Heating 3: 89 percent / CHCl3 / 2 h / Ambient temperature 4: 62 percent / K2CO3 / acetonitrile / 4.5 h / Heating 5: 80 percent / NaI, K2CO3 / acetonitrile / 15 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
66203-07-4
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 90 percent / HCl / ethanol / 20 h / Heating 3: 89 percent / CHCl3 / 2 h / Ambient temperature 4: 62 percent / K2CO3 / acetonitrile / 4.5 h / Heating 5: 22 percent / NaI, K2CO3 / acetonitrile / 15 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
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