2-(对二甲基氨基苯基)乙胺合成路线 （共 9 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 48 h;
参考文献
VIVALIS; GUEDAT, Philippe; BERECIBAR, Amaya; CIAPETTI, Paola; VENKATA PITHANI, Subhash; TROUCHE, Nathalie
Patent: WO2013/171281 A1, 2013 ;
Location in patent: Page/Page column 125-126 ;
反应条件
hydrazine in ethanol T=65°C; 5 h;
参考文献
ELAN PHARMACEUTICALS, INC.
Patent: WO2003/93245 A1, 2003 ;
Location in patent: Page/Page column 151 ;
WO 03/093245 A1
反应条件
hydrogenchloride in dichloromethane; ethyl acetate T=0 - 20°C;
参考文献
Hamada, Shohei; Kim, Tae-Dong; Suzuki, Takayoshi; Itoh, Yukihiro; Tsumoto, Hiroki; Nakagawa, Hidehiko; Janknecht, Ralf; Miyata, Naoki
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 10 p. 2852 - 2855
反应条件
methanol; ammonia; nickel T=120°C; P=51485.6 Torr; Hydrogenation;
参考文献
v.Braun; Blessing
Chemische Berichte, 1923 , vol. 56, p. 2160
反应条件
1: butylamine; acetic acid; ethanol 2: LiAlH4; diethyl ether View Scheme
参考文献
Vivalis; Guedat, Philippe; Berecibar, Amaya; Ciapetti, Paola; Venkata Pithani ,Subhash; Trouche, Nathalie
Patent: EP2664616 A1, 2013 ;
Title/Abstract Full Text Show Details
VIVALIS; GUEDAT, Philippe; BERECIBAR, Amaya; CIAPETTI, Paola; VENKATA PITHANI, Subhash; TROUCHE, Nathalie
Patent: WO2013/171281 A1, 2013 ;
反应条件
1: Na2CO3 2: Raney nickel; methanol; NH3 / 120 °C / 51485.6 Torr / Hydrogenation View Scheme
参考文献
Borovicka et al.
Chemicke Listy, 1955 , vol. 49, p. 231,241
Collection of Czechoslovak Chemical Communications, 1955 , vol. 20, p. 437,449
Chem.Abstr., 1956 , p. 1639,1640
反应条件
ueber das Saeurechlorid und -azid;
参考文献
Ashley; Leeds
Journal of the Chemical Society, 1957 , p. 2706,2710
参考文献
v.Braun; Blessing
Chemische Berichte, 1923 , vol. 56, p. 2160
参考文献
v.Braun; Blessing
Chemische Berichte, 1923 , vol. 56, p. 2160
