1,4,7,10-四甲苯磺酰-1,4,7,10-四氮杂环十二烷合成路线 (共 22 条)
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in water; toluene 9 h; Heating;
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in water; toluene Heating8-10 h;
参考文献
Luk'yanenko, N. G.; Basok, S. S.; Filonova, L. K.; Kulikov, N. V.; Pastushok, V. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 3 p. 346 - 349
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 3 p. 401 - 404
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; 30 h;
参考文献
Das, Tapas; Chakraborty, Sudipta; Banerjeel, Sharmila; Samuel, Grace; Sarma; Venkatesh, Meera; Pillai
Journal of Labelled Compounds and Radiopharmaceuticals, 2003 , vol. 46, # 3 p. 197 - 209
反应条件
potassium carbonate in acetonitrile 144 h; Heating;
参考文献
Pulacchini, Sonia; Watkinson, Michael
European Journal of Organic Chemistry, 2001 , # 22 p. 4233 - 4238
反应条件
caesium carbonate in acetonitrile T=80°C; 48 h;
参考文献
Kohl, Stephan W.; Kuse, Katharina; Hummert, Markus; Schumann, Herbert; Muegge, Clemens; Janek, Katharina; Weisshoff, Hardy
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2007 , vol. 62, # 3 p. 397 - 406
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Iwata, Masaaki; Kuzuhara, Hiroyoshi
Journal of the Chemical Society, Chemical Communications, 1985 , # 13 p. 918 - 919
反应条件
in N,N-dimethyl-formamide T=50°C;
参考文献
Iwata, Masaaki; Kuzuhara, Hiroyoshi
Chemistry Letters, 1986 , p. 369 - 372
反应条件
in N,N-dimethyl-formamide 1 h; Heating;
参考文献
Swinkels, Dorine W.; Duynhoven, John P. M. van; Hilbers, Cornelis W.; Tesser, Godefridus I.
Recueil des Travaux Chimiques des Pays-Bas, 1991 , vol. 110, # 4 p. 124 - 128
反应条件
in N,N-dimethyl-formamide T=120°C; microwave irradiation;
参考文献
Jebasingh; Alexander
Synthetic Communications, 2006 , vol. 36, # 5 p. 653 - 657
反应条件
1: 97 percent / Et3N / acetonitrile / 5 h / 20 °C 2: 78 percent / K2CO3 / dimethylformamide / 30 h / 100 °C View Scheme
参考文献
Meunier, I.; Mishra, A. K.; Hanquet, B.; Cocolios, P.; Guilard, R.
Canadian Journal of Chemistry, 1995 , vol. 73, # 5 p. 685 - 695