反应条件
in neat (no solvent) Ar-atmosphere; stirring tetrahexenylgermane, Et3GeH and GeCl4 (room temp., 3 d), distn. off of Et3GeCl, dissoln. in THF, addn. to excess Grignard reagent, boiling for 5 h; can be purified by chromy. (Ni-impregnated SiO2, pentane);
参考文献
Journal of Organometallic Chemistry, , vol. 521, # 1-2 p. 253 - 260