1,2,3,5-四甲基苯合成路线 （共 148 条）
反应条件
1: With titanium tetrachloride in dichloromethane T=-78 - -40°C; 2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
参考文献
Peron, Guillaume; Norton, David; Kitteringham, John; Kilburn, Jeremy D.
Tetrahedron Letters, 2001 , vol. 42, # 2 p. 347 - 349
反应条件
triethylsilane; aluminium trichloride in dichloromethane T=18 - 20°C; 1 h;
参考文献
Bolestova, G. I.; Shevchenko, N. V.; Parnes, Z. N.; Vol'pin, M. E.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 12.2 p. 2224 - 2227
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 12 p. 2565 - 2570
反应条件
palladium diacetate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in methanol; water T=80°C; 12 h; Inert atmosphere;
参考文献
Yamamoto, Yasunori; Ikizakura, Kazuya; Ito, Hajime; Miyaura, Norio
Molecules, 2013 , vol. 18, # 1 p. 430 - 439
反应条件
isopropyl alcohol; InI3 T=200°C; 2 - 3 h;
参考文献
CALIFORNIA INSTITUTE OF TECHNOLOGY; BP CHEMICALS LIMITED
Patent: WO2008/24896 A2, 2008 ;
Location in patent: Page/Page column 19-20; 25-26 ;
参考文献
Taher, Deeb; Thibault, Michelle E.; Di Mondo, Domenico; Jennings, Michael; Schlaf, Marcel
Chemistry - A European Journal, 2009 , vol. 15, # 39 p. 10132 - 10143
反应条件
aluminium trichloride T=70 - 75°C;
参考文献
McCaulay; Lien
Journal of the American Chemical Society, 1952 , vol. 74, p. 6246,6248
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(l) iodide; trifluoroacetic acid sodium salt T=150 - 180°C; 15 h;
参考文献
Suzuki, Hitomi; Yoshida, Yoshiki; Osuka, Atsuhiro
Chemistry Letters, 1982 , p. 135 - 136
反应条件
titanium tetrachloride in dichloromethane T=-78 - -40°C;
参考文献
Peron, Guillaume; Norton, David; Kitteringham, John; Kilburn, Jeremy D.
Tetrahedron Letters, 2001 , vol. 42, # 2 p. 347 - 349
反应条件
isopropyl alcohol; zinc(II) iodide T=200°C; 2 - 3 h;
参考文献
CALIFORNIA INSTITUTE OF TECHNOLOGY; BP CHEMICALS LIMITED
Patent: WO2008/24896 A2, 2008 ;
Location in patent: Page/Page column 19-20; 25-26 ;
反应条件
carbon monoxide; hydrogen; benzene T=190°C; Reagens 4: Octacarbonyldikobalt; Reagens 5: CoCO3;
参考文献
Wender et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4079,4082
