1,2,3,5-四甲基苯合成路线 （共 148 条）
反应条件
aluminium trichloride
T=50°C; 2 h;
参考文献
Andreou et al.
Tetrahedron, 1980 , vol. 36, p. 2101
参考文献
Gray; Walker; Fuson
Journal of the American Chemical Society, 1931 , vol. 53, p. 3494,3496
反应条件
aluminium trichloride
T=160°C; 3 h;
参考文献
El-Khawaga, Ahmed M.; Roberts, Royston M.
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3832 - 3834
反应条件
aluminium trichloride
T=100°C; 6 h;
参考文献
El-Khawaga, Ahmed M.; Roberts, Royston M.
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3832 - 3834
反应条件
1: 12 percent / AlCl3 / 6 h / 100 °C
2: 80 percent / AlCl3 / 3 h / 160 °C
View Scheme
参考文献
El-Khawaga, Ahmed M.; Roberts, Royston M.
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3832 - 3834
反应条件
1: AlCl3 / CS2
2: LiAlH4 / diethyl ether
View Scheme
参考文献
Newman,M.S. et al.
Journal of the American Chemical Society, 1964 , vol. 86, p. 868 - 872
反应条件
chlorosulfonic acid
1.) -5 deg C, 2.) RT, reduced preassure;
参考文献
Sekine, Mitsuo; Matsuzaki, Jun-Ichi; Hata, Tsujiaki
Tetrahedron, 1985 , vol. 41, # 22 p. 5279 - 5288
参考文献
Smith; Cass
Journal of the American Chemical Society, 1932 , vol. 54, p. 1609,1611
参考文献
Smith; Cass
Journal of the American Chemical Society, 1932 , vol. 54, p. 1609,1611
Full Text Show Details
Moyle; Smith
Journal of Organic Chemistry, 1937 , vol. 2, p. 112,116, 132
反应条件
tris-(2-chloro-ethyl)-amine; trifluorormethanesulfonic acid; trifluoroacetic acid in chloroform
T=25°C; 1 h;
参考文献
Takeuchi, Hiroshi; Adachi, Taki; Nishiguchi, Hideaki; Itou, Katsutaka; Koyama, Kikuhiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 7 p. 867 - 870
