2,6-二甲基-2,5-环己二烯-1,4-二酮合成路线 （共 148 条）
反应条件
cyclohepta-1,3,5-triene in toluene 1.5 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 7 p. 2072 - 2077
反应条件
sodium acetate in methanol; water T=24°C; further compound; Equilibrium constant;
参考文献
Brown,E.R. et al.
Journal of Organic Chemistry, 1971 , vol. 36, # 19 p. 2849 - 2853
反应条件
sodium acetate in methanol; water T=24°C; Equilibrium constant;
参考文献
Brown,E.R. et al.
Journal of Organic Chemistry, 1971 , vol. 36, # 19 p. 2849 - 2853
反应条件
in toluene 1.5 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 7 p. 2072 - 2077
反应条件
in water T=24°C; UV-irradiation; Quantum yield; Further Variations:Solvents;
参考文献
Goerner, Helmut
Journal of Physical Chemistry A, 2003 , vol. 107, # 51 p. 11587 - 11595
反应条件
ether, THF, -78 deg C; 60 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Fischer, A.; Henderson, N.
Tetrahedron Letters, 1980 , vol. 21, p. 701 - 704
反应条件
1: hydrogen / Pd/Al2O3 / tert-butyl methyl ether / 1 h / 40 °C / 4500.45 Torr 2: tert-butyl methyl ether / 6 h / 60 °C / Inert atmosphere 3: hydrogen / 5 palladium on charcoal / tert-butyl methyl ether / 7 h / 140 °C / 8250.83 Torr / autoclave View Scheme
参考文献
DSM IP Assets B.V.; BONRATH, Werner; NETSCHER, Thomas; SCHUeTZ, Jan; WUeSTENBERG, Bettina
Patent: WO2012/25587 A1, 2012 ;
反应条件
acetic acid in water 264 h;
参考文献
Goldstein, Stephen L.; McNelis, Edward
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1613 - 1620
反应条件
potassium cyanide; samarium diiodide; 18-crown-6 ether 1.) CH2Cl2, room t., 20 min, 2.) THF, MeOH, -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Olson, Steven H.; Danishefsky, Samuel J.
Tetrahedron Letters, 1994 , vol. 35, # 43 p. 7901 - 7904
反应条件
1: SnCl2; concentrated aqueous HCl 2: HCl; AlCl3; benzene / 60 °C / Behandeln des Reaktionsprodukts mit wss. HCl unter Durchleiten von Wasserdampf View Scheme
参考文献
Smith; Wiley
Journal of the American Chemical Society, 1946 , vol. 68, p. 887,890
Full Text Show Details
Smith; Johnson
Journal of the American Chemical Society, 1937 , vol. 59, p. 673,678
