2,6-二甲基-2,5-环己二烯-1,4-二酮合成路线 (共 148 条)
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate T=20°C; 0.583333 h;
参考文献
Yadav; Reddy; Swamy; Ramireddy
Synthesis, 2004 , # 11 p. 1849 - 1853
反应条件
trifluoroacetic acid in dichloromethane; water Ambient temperature;
参考文献
Bruce, J. Malcolm; Lloyd-Williams, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 21 p. 2877 - 2884
参考文献
Smith; Irwin
Journal of the American Chemical Society, 1941 , vol. 63, p. 1036,1040
反应条件
1: ethanolic sulfuric acid 2: sodium dithionite; aqueous ethanol View Scheme
参考文献
Smith; Irwin
Journal of the American Chemical Society, 1941 , vol. 63, p. 1036,1040
反应条件
1: 2,6-dimethyl-1,4-benzoquinone With zinc
2: methanol With sulfuric acid
参考文献
Paterson, Ian; Delgado, Oscar; Florence, Gordon J.; Lyothier, Isabelle; O'Brien, Matthew; Scott, Jeremy P.; Sereinig, Natascha
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 150 - 160
反应条件
1: sodium dithionite / methanol; water; diethyl ether / 1 h / 20 °C / |Inert atmosphere
2: sulfuric acid / methanol / 4 h / 100 °C
View Scheme
参考文献
Zhao, Wenjun; Huang, Li; Guan, Yong; Wulff, William D.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3436 - 3441
Angew. Chem., 2014 , vol. 126, # 13 p. 3504 - 3509,6
反应条件
10-methyl-9,10-dihydroacridine in acetonitrile
T=24.9°C; AcH2 as an acid stable NADH model: the effect of HClO4 and Mg(ClO4)2 on the rate constant of the hydride transfer reaction is measured; Rate constant;
参考文献
Fukuzumi, Shunichi; Ishikawa, Masashi; Tanaka, Toshio
Tetrahedron, 1986 , vol. 42, # 4 p. 1021 - 1034
反应条件
(i) Me3SiCN, KCN, 18-crown-6, (ii) /BRN= 3587162/, Et2O, (iii) aq. AgF, THF; Multistep reaction;
参考文献
Evans,D.A. et al.
Journal of the American Chemical Society, 1973 , vol. 95/17, p. 5822 - 5823
反应条件
1: sodium dithionite / methanol; water; diethyl ether / 1 h / 20 °C / |Inert atmosphere
2: sulfuric acid / 1.7 h / 20 °C / |Inert atmosphere
3: sodium dithionite; sodium hydroxide / water; ethanol / 0.67 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Zhao, Wenjun; Huang, Li; Guan, Yong; Wulff, William D.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3436 - 3441
Angew. Chem., 2014 , vol. 126, # 13 p. 3504 - 3509,6
反应条件
cyclohepta-1,3,5-triene in toluene
1.5 h; Heating;
参考文献
Mori, Akira; Mametsuka, Hiroaki; Takeshita, Hitoshi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 2072 - 2077