6-羟基-3,4-二氢-1H-2-萘酮合成路线 (共 5 条)
反应条件
boron trichloride; tetra-(n-butyl)ammonium iodide in dichloromethane T=-78 - 0°C; dealkylation; 1 h;
参考文献
Brooks, Paige R.; Wirtz, Michael C.; Vetelino, Michael G.; Rescek, Diane M.; Woodworth, Graeme F.; Morgan, Bradley P.; Coe, Jotham W.
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9719 - 9721
反应条件
aluminum tri-bromide; cyclohexane in various solvent(s) T=25°C; 72 h;
参考文献
Ostashevskaya; Koltunov; Repinskaya
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 10 p. 1474 - 1477
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=0°C; Friedel-Crafts reaction;
参考文献
Jetter, Michele C.; Youngman, Mark A.; McNally, James J.; McDonnell, Mark E.; Zhang, Sui-Po; Dubin, Adrienne E.; Nasser, Nadia; Codd, Ellen E.; Flores, Christopher M.; Dax, Scott L.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 22 p. 6160 - 6163
反应条件
dihydrogen peroxide; hydrogen fluoride; SbF5 T=-50°C; 0.0333333 h; MechanismProduct distribution;
参考文献
Gesson, Jean-Pierre; Jacquesy, Jean-Claude; Jouannetaud, Marie-Paule; Morellet, Guy
Tetrahedron Letters, 1983 , vol. 24, # 30 p. 3095 - 3098
反应条件
glucose dehydrogenase; D-glucose; tetrahydroxynaphthalene reductase; β-NADP in isopropyl alcohol pH=7; KPi bufferInert atmosphereEnzymatic reaction;
参考文献
Schaetzle, Michael A.; Flemming, Stephan; Husain, Syed Masood; Richter, Michael; Guenther, Stefan; Mueller, Michael
Angewandte Chemie - International Edition, 2012 , vol. 51, # 11 p. 2643 - 2646