顺式-2,4,5-三甲氧基-1-丙烯基苯合成路线 (共 20 条)
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
参考文献
Angewandte Chemie, , vol. 95, # 8 p. 629 - 630
反应条件
silica gel in 1,4-dioxane 0.05 h; microwave irradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 12 p. 2231 - 2235
反应条件
potassium carbonate in 1,4-dioxane Wittig reaction; 24 h; Heating; Title compound not separated from byproducts.;
参考文献
Organic Preparations and Procedures International, , vol. 39, # 5 p. 514 - 517
反应条件
1: With potassium carbonate in 1,4-dioxane Wittig reaction; 24 h; Heating; 2: With dichloro bis(acetonitrile) palladium(II) in dichloromethane T=20°C; 24 h; Further stages.;
参考文献
Organic Preparations and Procedures International, , vol. 39, # 5 p. 514 - 517
反应条件
1.1: magnesium / diethyl ether / 2 h 1.2: 78 percent / diethyl ether; toluene / 20 °C 2.1: silica gel / dioxane / 0.05 h / microwave irradiation View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 12 p. 2231 - 2235
反应条件
potassium hydroxide in ethanol
参考文献
Canadian Journal of Chemistry, , vol. 43, p. 3437 - 3440
参考文献
Archiv der Pharmazie, , vol. 315, # 6 p. 571 - 574
反应条件
sodium periodate; osmium(VIII) oxide; N-benzyl-N,N,N-triethylammonium chloride in tetrahydrofuran; water T=100°C; Microwave irradiation;
参考文献
Kumar, Rakesh; Mohanakrishnan, Dinesh; Sharma, Abhishek; Kaushik, Naveen Kumar; Kalia, Kalpana; Sinha, Arun Kumar; Sahal, Dinkar
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 11 p. 5292 - 5301
反应条件
sodium periodate; OsO4
参考文献
Sinha, Arun Kumar; Joshi, Bhupendra Prasad; Dogra, Ruchi
Patent: US2002/153240 A1, 2002 ;
反应条件
720 h; Irradiation; Further byproducts given;
参考文献
Saxena, D. B.; Mukerjee, S. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 683 - 684