反应条件
1: N-ethyl-N,N-diisopropylamine / 2-methyl tetrahydrofuran / 0.5 h / 80 °C / Large scale reaction
2: iron; ammonium chloride / water; N,N-dimethyl-formamide / 1.67 h / 20 - 100 °C / Large scale reaction
View Scheme
参考文献
Giubellina, Nicola; Stabile, Paolo; Laval, Gilles; Perboni, Alcide D.; Cimarosti, Zadeo; Westerduin, Pieter; Cooke, Jason W. B.
Organic Process Research and Development, 2010 , vol. 14, # 4 p. 859 - 867