2-乙酰基-5-硝基呋喃合成路线 (共 24 条)
反应条件
1: 54 percent / sulfuric acid / acetic acid / 48 h / Ambient temperature
2: 58 percent / bromine / CHCl3 / Ambient temperature
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参考文献
Tulecki, Jerzy; Sobiak, Stanislaw
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1559 - 1562
反应条件
1: 36 percent / sulfuric acid / acetic acid / 48 h / Ambient temperature
2: 50 percent / bromine / CHCl3 / Ambient temperature
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参考文献
Tulecki, Jerzy; Sobiak, Stanislaw
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1559 - 1562
反应条件
1: 28 percent / sulfuric acid / acetic acid / 48 h / Ambient temperature
2: 35 percent / bromine / CHCl3 / Ambient temperature
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参考文献
Tulecki, Jerzy; Sobiak, Stanislaw
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1559 - 1562
反应条件
1: 63 percent / sulfuric acid / acetic acid / 48 h / Ambient temperature
2: 63 percent / bromine / CHCl3 / Ambient temperature
View Scheme
参考文献
Tulecki, Jerzy; Sobiak, Stanislaw
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1559 - 1562
反应条件
1: 63 percent / sulfuric acid / acetic acid / 48 h / Ambient temperature
2: 63 percent / bromine / CHCl3 / Ambient temperature
3: 39 percent / triethylamine / benzene / 24 h / Ambient temperature
View Scheme
参考文献
Tulecki, Jerzy; Sobiak, Stanislaw
Polish Journal of Chemistry, 1982 , vol. 56, # 10-12 p. 1559 - 1562
反应条件
1: Br2 / CHCl3
2: AcOH / 2 h
View Scheme
参考文献
Saldabol,N.O. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, # 5 p. 1598 - 1601,1608 - 1610
反应条件
iodine in N,N-dimethyl-formamide
参考文献
Saldabol,N.O.; Giller,S.A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1976 , vol. 12, p. 1155 - 1162
Khimiya Geterotsiklicheskikh Soedinenii, 1976 , vol. 12, p. 1396 - 1405
反应条件
iodine in N,N-dimethyl-formamide
参考文献
Saldabol,N.O.; Giller,S.A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1976 , vol. 12, p. 1155 - 1162
Khimiya Geterotsiklicheskikh Soedinenii, 1976 , vol. 12, p. 1396 - 1405
反应条件
iodine in N,N-dimethyl-formamide
参考文献
Saldabol,N.O.; Giller,S.A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1976 , vol. 12, p. 1155 - 1162
Khimiya Geterotsiklicheskikh Soedinenii, 1976 , vol. 12, p. 1396 - 1405
反应条件
bromine in N,N-dimethyl-formamide
参考文献
Saldabol,N.O.; Giller,S.A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1976 , vol. 12, p. 1155 - 1162
Khimiya Geterotsiklicheskikh Soedinenii, 1976 , vol. 12, p. 1396 - 1405