2-乙酰基-2-环己烯-1-酮合成路线 (共 7 条)
反应条件
iodosylbenzene in chloroform-d1
T=20°C; 12 h;
参考文献
McQuaid, Kevin M.; Pettus, Thomas R. R.
Synlett, 2004 , # 13 p. 2403 - 2405
反应条件
ozone in dichloromethane
参考文献
Reich,H.J. et al.
Journal of the American Chemical Society, 1975 , vol. 97, # 19 p. 5434 - 5447
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; copper dichloride in acetonitrile
T=75°C; P=9000.9 Torr; 5 h; Autoclave;
参考文献
Chen, Lihua; Tang, Ruiren; Li, Zhongying; Liang, Shan
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 2 p. 459 - 463
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran
T=-78°C; 0.166667 h;
2: With polymer-supported selenium bromide in tetrahydrofuran
T=-78 - 20°C; 0.75 h;
3: With dihydrogen peroxide in tetrahydrofuran
T=20°C; 0.5 h;
参考文献
Sheng, Shou-Ri; Liu, Xiao-Ling; Wang, Xing-Cong
Journal of the Chinese Chemical Society, 2003 , vol. 50, # 2 p. 279 - 281
反应条件
3-chloro-benzenecarboperoxoic acid
参考文献
Liotta, Dennis; Saindane, Manohar; Barnum, Christopher; Ensley, Harry; Balakrishnan, Pattabiraman
Tetrahedron Letters, 1981 , vol. 22, # 32 p. 3043 - 3046
反应条件
iron(II) chloride
T=-10 - -5°C; electrolysis (undivided cell, Pt-anode, Cu-cathode);
参考文献
Vukicevic, Rastko D.; Joksovic, Ljubinka; Konstantinovic, Stanimir; Markovic, Zoran; Mihailovic, Mihailo Lj.
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 4 p. 899 - 904
反应条件
tetraethylammonium chloride in dichloromethane
T=15 - 18°C; electrolysis with Al- or C-anode and Cu-cathode; var. electrolyte medium, other temp., also acetic anhydride as acylating agent; Product distribution;
参考文献
Vukicevic, Rastko; Konstantinovic, Stanimir; Joksovic, Ljubinka; Ponticelli, Gustavo; Mihailovic, Mihailo Lj.
Chemistry Letters, 1995 , # 4 p. 275 - 276