phenyllithium in diethyl ether dropwise addn. of epoxyethyl(triphenyl)tin in ether to PhLi in ether (temp.: -78°C); quenching with water and CH2Cl2, drying of org. layer, concn. of org. layer, pptn.;
参考文献
Journal of Organometallic Chemistry, , vol. 341, p. 293 - 314