4'-甲氧基-N-甲基甲酰苯胺合成路线 (共 20 条)
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) in tert-butyl alcohol
T=110°C; 24 h;
参考文献
Ikawa, Takashi; Barder, Timothy E.; Biscoe, Mark R.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2007 , vol. 129, # 43 p. 13001 - 13007
反应条件
potassium phosphate; copper(l) iodide; (1S,2S)-1,2-diaminocyclohexane in 1,4-dioxane
T=110°C; 23 h;
参考文献
Klapars, Artis; Huang, Xiaohua; Buchwald, Stephen L.
Journal of the American Chemical Society, 2002 , vol. 124, # 25 p. 7421 - 7428
反应条件
potassium phosphate; CuI in 1,4-dioxane; N-dodecane; ethyl acetate
参考文献
Buchwald, Stephen L.; Klapars, Artis; Antilla, Jon C.; Job, Gabriel E.; Wolter, Martina; Kwong, Fuk Y.; Nordmann, Gero; Hennessy, Edward J.
Patent: US2003/65187 A1, 2003 ;
反应条件
T=20°C; 0.0333333 h; Green chemistry;
参考文献
Habibi, Davood; Nasrollahzadeh, Mahmoud
Comptes Rendus Chimie, 2013 , vol. 16, # 11 p. 1008 - 1016
参考文献
Kim, Joong-Gon; Jang, Doo Ok
Synlett, 2010 , # 14 art. no. U04610ST, p. 2093 - 2096
反应条件
oxygen; iron(III) chloride in acetonitrile
T=50°C; P=760 Torr; 16 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1297 - 1298
反应条件
potassium fluoride on basic alumina in acetonitrile
T=20°C; 24 h;
参考文献
Mihara, Masatoshi; Ishino, Yoshio; Minakata, Satoshi; Komatsu, Mitsuo
Synthesis, 2003 , # 15 p. 2317 - 2320
反应条件
sodium hydroxide in ethanol; water
T=27°C; 9 h;
参考文献
Preedasuriyachai, Patcharee; Kitahara, Hiroaki; Chavasiri, Warinthorn; Sakurai, Hidehiro
Chemistry Letters, 2010 , vol. 39, # 11 p. 1174 - 1176
反应条件
oxygen in acetonitrile
T=30°C; 5 h;
参考文献
Murata, Satoru; Tamatani, Akira; Suzuki, Kaoru; Miura, Masahiro; Nomura, Masakatsu
Chemistry Letters, 1990 , # 5 p. 757 - 760
反应条件
Benzoyl cyanide; oxygen; iron(III) chloride in acetonitrile
T=50°C; P=760 Torr; 16 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1297 - 1298