4'-甲氧基-N-甲基甲酰苯胺合成路线 (共 20 条)
反应条件
palladium diacetate; sodium acetate in acetic acid; benzene
T=80°C; 5 h; Further byproducts given;
参考文献
Sakakibara, Tsutomu; Hamakawa, Tomoko
Chemistry Letters, 1982 , p. 1823 - 1824
反应条件
oxygen; acetic anhydride in acetonitrile
T=30°C; 5 h;
参考文献
Murata, Satoru; Tamatani, Akira; Suzuki, Kaoru; Miura, Masahiro; Nomura, Masakatsu
Chemistry Letters, 1990 , # 5 p. 757 - 760
反应条件
palladium diacetate; sodium acetate in acetic acid; benzene
T=80°C; 5 h; Further byproducts given;
参考文献
Sakakibara, Tsutomu; Hamakawa, Tomoko
Chemistry Letters, 1982 , p. 1823 - 1824
参考文献
Deutsch; Niclas
Synthetic Communications, 1993 , vol. 23, # 11 p. 1561 - 1568
反应条件
oxygen; copper dichloride in acetonitrile
T=50°C; 20 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Journal of Chemical Research, Miniprint, 1993 , # 10 p. 2827 - 2840
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate in benzene
T=5 - 10°C; 1 h; Heating;
参考文献
Sharma, V. K.; Kumar, A.; Agarwal, K. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 11 p. 1153
反应条件
sulfuric acid
Heating;
参考文献
Meth-Cohn, Otto; Taylor, David L.
Tetrahedron, 1995 , vol. 51, # 47 p. 12869 - 12882
反应条件
1: benzene / Heating
2: anhydrous potassium carbonate, sodium hydroxide, tetrabutylammonium hydrogensulphate / benzene / 1 h / 5 - 10 °C / Heating
View Scheme
参考文献
Sharma, V. K.; Kumar, A.; Agarwal, K. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 11 p. 1153
反应条件
in chloroform-d1
1 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hoffman, Robert V.; Salvador, James M.
Journal of Organic Chemistry, 1992 , vol. 57, # 16 p. 4487 - 4490
反应条件
in ethanol
1 h; Irradiation; Quantum yield;
参考文献
Ogata, Yoshiro; Tagaki, Katsuhiko; Mizuno, Kiyohiko
Journal of Organic Chemistry, 1982 , vol. 47, p. 3684 - 3687