3-(1H-吲哚-3-基)-3-氧丙酸乙酯合成路线 （共 6 条）
参考文献
Majima; Shigematsu; Rokkaku
Chemische Berichte, 1924 , vol. 57, p. 1455
Full Text Show Details
Baker
Journal of the Chemical Society, 1940 , p. 462,463
反应条件
1: With trifluoroacetic acid in dichloromethane
0.5 h; Reflux;
2: With water; silica gel
参考文献
Yu, Haifeng; Yu, Zhengkun
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 2929 - 2933
Angewandte Chemie, 2009 , vol. 121, p. 2973 - 2977
反应条件
diethylaluminium chloride in hexane; dichloromethane
T=0°C; 2 h;
参考文献
Conchon, Elisabeth; Aboab, Bettina; Golsteyn, Roy M.; Cruzalegui, Francisco; Edmonds, Thomas; Leonce, Stephane; Pfeiffer, Bruno; Prudhomme, Michelle
European Journal of Medicinal Chemistry, 2006 , vol. 41, # 12 p. 1470 - 1477
参考文献
Majima; Shigematsu; Rokkaku
Chemische Berichte, 1924 , vol. 57, p. 1455
Full Text Show Details
Oddo; Albanese
Gazzetta Chimica Italiana, 1927 , vol. 57, p. 827,830
反应条件
in methanol
Electrochemical reduction at pH 6 - 7, a mercury cathode and a platinum anode.;
参考文献
Vinograd, L. Kh.; Sorokina, N. P.; Turchin, K. F.; Dubinskii, R. A.; Suvorov, N. N.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 12 p. 2222 - 2226
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2594 - 2599
反应条件
magnesium; ethyl iodide
1) Ether, boiling, 1.5 h, 2) 5 deg C, 10 min.; Yield given. Multistep reaction;
参考文献
Vinograd, L. Kh.; Sorokina, N. P.; Turchin, K. F.; Dubinskii, R. A.; Suvorov, N. N.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 12 p. 2222 - 2226
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 12 p. 2594 - 2599
