反应条件
1: trimethyl cyclohexane-1,3,5-tricarboxylate With n-butyllithium; diisopropylamine in diethyl ether; hexane
T=0°C; 2 h;
2: dimethyl sulfate in diethyl ether; hexane
T=20°C;
参考文献
Ye, Qing; Komarov, Igor V.; Kirby, Anthony J.; Jones Jr., Maitland
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9288 - 9294