反应条件
in tetrahydrofuran; diethyl ether
Ar atmosphere, addn. of Al compd. to soln. of Si compd. (-23°C, 0.5 h), refluxing (9 h), cooling (0°C), addn. of MeLi soln., stirring (room temp.), addn. of solns. (THF) of Cu complex and Me3SnCl, cooling, warming, extn. (Et2O); washing (water), drying, hexane addn., filtration, chromy. (silica gel, hexane);
参考文献
Rossi, Renzo; Carpita, Adriano; Bellina, Fabio; De Santis, Massimo; Veracini, Carlo Alberto
Gazzetta Chimica Italiana, 1990 , vol. 120, p. 457 - 464
