环己基 beta-D-吡喃葡萄糖苷合成路线 （共 13 条）
反应条件
immobilized β-glucosidase G 0395 from almonds (EC 3.2.1.21) in water
T=20°C; 144 h;
参考文献
Balogh, Terez; Boross, Laszlo; Kosary, Judit
Tetrahedron, 2004 , vol. 60, # 3 p. 679 - 682
反应条件
palladium on activated charcoal; hydrogen
T=20°C; 24 h; Overall yield = 87 percent;
参考文献
Ishihara, Masaki; Takagi, Yuka; Li, Gefei; Noguchi, Masato; Shoda, Shin-Ichiro
Chemistry Letters, 2013 , vol. 42, # 10 p. 1235 - 1237
反应条件
Amberlyst A-26 in methanol
T=20°C; 3 h;
参考文献
Ackermann, Irmtraud E.; Banthorpe, Derek V.; Fordham, William D.; Kinder, John P.; Poots, Ian
Liebigs Annalen der Chemie, 1989 , p. 79 - 82
反应条件
scandium tris(trifluoromethanesulfonate)
T=80°C; 3 h; Ionic liquid; optical yield given as percent dediastereoselective reaction;
参考文献
Auge, Jacques; Sizun, Gwenaelle
Green Chemistry, 2009 , vol. 11, # 8 p. 1179 - 1183
反应条件
Pyrococcus furiosus β-glucosidase/gelatin-gel
T=70°C; pH=5; 12 h; citrate bufferEnzymatic reaction;
参考文献
Matsushita, Yoh-Ichi; Nagatomo, Hidetaka; Sugamoto, Kazuhiro; Matsui, Takanao
Letters in Organic Chemistry, 2009 , vol. 6, # 2 p. 115 - 119
反应条件
β-galactosidase in water
T=35°C; 4 h; phosphate buffer (pH 5);
参考文献
Ooi, Yasuhiro; Hashimoto, Toshihiro; Mitsuo, Naoki; Satoh, Toshio
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 4 p. 1808 - 1814
反应条件
1: NaOMe / methanol
2: mercuric nitrate / acetonitrile
View Scheme
参考文献
Hanessian, Stephen; Bacquet, Christian; Lehong, Nghiep
Carbohydrate Research, 1980 , vol. 80, p. C17 - C22
反应条件
1: 86 percent / potassium carbonate / acetone; toluene / 1 h
2: NaOMe / methanol
3: mercuric nitrate / acetonitrile
View Scheme
参考文献
Hanessian, Stephen; Bacquet, Christian; Lehong, Nghiep
Carbohydrate Research, 1980 , vol. 80, p. C17 - C22
反应条件
gold(III) chloride in acetonitrile
4 h; RefluxInert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Mamidyala, Sreeman K.; Finn
Journal of Organic Chemistry, 2009 , vol. 74, # 21 p. 8417 - 8420
反应条件
Hg(NO3)2 in acetonitrile
参考文献
Hanessian, Stephen; Bacquet, Christian; Lehong, Nghiep
Carbohydrate Research, 1980 , vol. 80, p. C17 - C22
