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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
52843-75-1
合成路线
（共 9 条）
52843-75-1
+
13922-41-3
1-萘硼酸
→
反应条件
189193-21-3
反应条件
potassium phosphate; C58H72N2O4P2Pd2 in tert-butyl alcohol T=110°C; Suzuki-Miyaura cross-coupling; 3 h; Inert atmosphere;
参考文献
So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Angewandte Chemie - International Edition, 2008 , vol. 47, # 42 p. 8059 - 8063
905966-46-3
+
52843-75-1
→
反应条件
21308-81-6
3-(3-噻吩)吡啶
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 14 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
52843-75-1
+
1314538-55-0
[(叔丁氧羰基氨基)甲基]三氟硼酸钾
→
反应条件
102297-41-6
N-Boc-3-氨甲基吡啶
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; dichloro(cycloocta-1,5-diene)palladium(II) in water; tert-butyl alcohol T=95°C; Suzuki-Miyaura cross-coupling; 22 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 12 p. 3138 - 3141
52843-75-1
+
98-80-6
苯硼酸
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
potassium phosphate; (NC5H3(N2C7H4(CH2)3CH3)2)NiBr(1+)*Br(1-)=Ni(NC5H3(N2C7H4(CH2)3CH3)2)Br2; triphenylphosphine in 1,4-dioxane T=100°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Tu, Tao; Mao, Han; Herbert, Christian; Xu, Mizhi; Doetz, Karl Heinz
Chemical Communications, 2010 , vol. 46, # 41 p. 7796 - 7798
52843-75-1
+
355408-55-8
噻吩-2-硼酸新戊二醇酯
→
反应条件
21298-53-3
3-(2-噻吩基)吡啶
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
905966-40-7
+
52843-75-1
→
反应条件
90395-47-4
4-(3-吡啶)苯甲酸甲酯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
52843-75-1
+
17873-01-7
三甲氧基(对甲苯基)硅烷
→
反应条件
4423-09-0
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; tert-butyl alcohol T=90°C; Hiyama coupling; Inert atmosphere;
参考文献
Zhang, Liang; Qing, Jiang; Yang, Pengyuan; Wu, Jie
Organic Letters, 2008 , vol. 10, # 21 p. 4971 - 4974
52843-75-1
+
213596-33-9
→
反应条件
5958-02-1
3-(4-甲氧基苯基)吡啶
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
52843-75-1
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5958-02-1
3-(4-甲氧基苯基)吡啶
反应条件
anhydrous dipotassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling reaction; Inert atmosphere;
参考文献
Gao, Han; Li, You; Zhou, Yi-Guo; Han, Fu-She; Lin, Ying-Jie
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 309 - 314
