1,6-二叠氮基-1,6-二脱氧-D-甘露醇合成路线 （共 5 条）
反应条件
1: With sodium azide in N,N-dimethyl-formamide
T=130°C; 0.25 h;
2: With sodium methylate in methanol
T=20°C; 24 h;
参考文献
Glacon, Virginie; Benazza, Mohammed; Anzi, Aniss; Beaupere, Daniel; Demailly, Gilles
Journal of Carbohydrate Chemistry, 2004 , vol. 23, # 2-3 p. 95 - 110
反应条件
hydrogenchloride; water
T=20°C; 20 h;
参考文献
Ferreira, Marcelle de L.; Vasconcelos, Thatyana R.A.; de Carvalho, Erika M.; Lourenco, Maria C.S.; Wardell, Solange M.S.V.; Wardell, James L.; Ferreira, Vitor F.; de Souza, Marcus V.N.
Carbohydrate Research, 2009 , vol. 344, # 15 p. 2042 - 2047
反应条件
sodium azide in N,N-dimethyl-formamide
T=90°C; 2 h;
参考文献
Glacon, Virginie; Benazza, Mohammed; Anzi, Aniss; Beaupere, Daniel; Demailly, Gilles
Journal of Carbohydrate Chemistry, 2004 , vol. 23, # 2-3 p. 95 - 110
反应条件
potassium hydroxide in ethanol
T=0°C; 24 h;
参考文献
Boularand; Kamdem; Imbach; et al.
1973 , vol. 8, # 6 p. 638 - 646
反应条件
1: NaN3 / dimethylformamide / 48 h / 60 - 70 °C
2: aq. KOH / ethanol / 24 h / 0 °C
View Scheme
参考文献
Boularand; Kamdem; Imbach; et al.
1973 , vol. 8, # 6 p. 638 - 646
