1: With sodium hydroxide in water T=100°C; 0.0166667 h; microwave irradiation; 2: With mercury(II) diacetate in water T=180°C; Pesci reaction; 0.25 h; microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.25 h; microwave irradiation; Title compound not separated from byproducts;

water; mercury(II) oxide T=150°C; Erhitzen des Reaktionsprodukts mit wss. Salzsaeure;

1: With sodium hydroxide in water T=100°C; 0.0166667 h; microwave irradiation; 2: With mercury(II) diacetate in water T=180°C; Pesci reaction; 0.25 h; microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.25 h; microwave irradiation; Title compound not separated from byproducts;

1: 1 h / 160 °C 2: LiAlH4 / toluene; diethyl ether / 22 h / 50 °C 3: H2 / 10percent Pd/C / aq. ethanol / 3 h / 2062.7 Torr View Scheme

in ethanol 2 h; Ambient temperature;

in ethanol 2 h; Ambient temperature;

Multistep reaction. Title compound not separated from byproducts;