3-溴-4,5-二羟基苄醇合成路线 (共 3 条)
反应条件
sodium tetrahydroborate in methanol
参考文献
Sudalai, A.; Rao, G. S. Krishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 858 - 859
反应条件
1: 80 percent / 48percent aq. HBr, glacial acetic acid / 3 h / Heating
2: 88 percent / NaBH4 / methanol
View Scheme
参考文献
Sudalai, A.; Rao, G. S. Krishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 1-11 p. 858 - 859
反应条件
1: Br2; AcOH / 0.5 h / 20 °C
2: KBH4
View Scheme
参考文献
Shoeib, Nagwa A.; Bibby, Michael C.; Blunden, Gerald; Linley, Peter A.; Swaine, David J.; Wheelhouse, Richard T.; Wright, Colin W.
Journal of Natural Products, 2004 , vol. 67, # 9 p. 1445 - 1449