N-(4-烯丁基)邻苯二甲酰亚胺合成路线 （共 22 条）
反应条件
in benzene 12 h; Heating;
参考文献
Harding, Kenn E.; Nam, Do-hyun
Tetrahedron Letters, 1988 , vol. 29, # 31 p. 3793 - 3796
反应条件
potassium carbonate in acetonitrile 12 h; Reflux;
参考文献
Lipshutz, Bruce H.; Ghorai, Subir; Leong, Wendy Wen Yi
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2854 - 2857
反应条件
tributylphosphine; ammonium formate; tris(dibenzylideneacetone)dipalladium (0) in toluene T=100°C; Reduction; Isomerization;
参考文献
Hughes, Gregory; Lautens, Mark; Wu, Jingxiao
Synlett, 2000 , # 6 p. 835 - 837
反应条件
1: With triphenylphosphine in tetrahydrofuran 2: With di-isopropyl azodicarboxylate in tetrahydrofuran T=0 - 20°C;
参考文献
Malkov, Andrei V.; Derrien, Nolwenn; Barlog, Maciej; Kocovsky, Pavel
Chemistry - A European Journal, 2014 , vol. 20, # 16 p. 4542 - 4547
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; 1 h;
参考文献
Ali, Ibrahim A. I.; El Ashry, El Sayed H.; Schmidt, Richard R.
Tetrahedron, 2004 , vol. 60, # 22 p. 4773 - 4780
反应条件
1: phthalimidomethyl iodide With copper(l) iodide; diethylzinc in hexane; dichloromethane T=20°C; 2 h; Inert atmosphere; 2: allyl bromide in hexane; dichloromethane T=20°C; 4 h; Inert atmosphere;
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
反应条件
in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
Jiranusornkul, Supat; Sirithunyalug, Busaban; Nemoto, Hideo; Takahata, Hiroki
Heterocycles, 2002 , vol. 56, # 1-2 p. 487 - 496
反应条件
in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Kanoh, Shigeyoshi; Naka, Masashi; Nishimura, Tomonari; Motoi, Masatoshi
Tetrahedron, 2002 , vol. 58, # 35 p. 7049 - 7064
反应条件
in N,N-dimethyl-formamide 1) 80 deg C, 3 h; 2) RT, 3 h;
参考文献
Machida, Minoru; Oda, Kazuaki; Kanaoka, Yuichi
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 75 - 84
反应条件
1: 71 percent / tetrahydrofuran; dimethylformamide / 2 h / -78 - 23 °C 2: 95 percent / HCO2NH4; n-Bu3P / Pd2(dba)3 / toluene / 100 °C View Scheme
参考文献
Synlett, , # 6 p. 835 - 837
