N-(4-烯丁基)邻苯二甲酰亚胺合成路线 （共 22 条）
反应条件
1.1: water / 4 h / 100 °C 2.1: thionyl chloride / 4 h / 75 °C / Inert atmosphere 3.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 4.1: copper(l) iodide; diethylzinc / hexane; dichloromethane / 2 h / 20 °C / Inert atmosphere 4.2: 4 h / 20 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 11 p. 3241 - 3247
反应条件
1.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 2.1: copper(l) iodide; diethylzinc / hexane; dichloromethane / 2 h / 20 °C / Inert atmosphere 2.2: 4 h / 20 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 11 p. 3241 - 3247
反应条件
1.1: thionyl chloride / 4 h / 75 °C / Inert atmosphere 2.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 3.1: copper(l) iodide; diethylzinc / hexane; dichloromethane / 2 h / 20 °C / Inert atmosphere 3.2: 4 h / 20 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 11 p. 3241 - 3247
反应条件
bis(benzonitrile)palladium(II) dichloride; AgNO2; CuCl2·2H2O; nitromethane; oxygen; tert-butyl alcohol T=20°C; Wacker Oxidation; P=760.051 Torr; 6 h;
参考文献
Wickens, Zachary K.; Morandi, Bill; Grubbs, Robert H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 43 p. 11257 - 11260
Angew. Chem., 2013 , vol. 125, # 43 p. 11467 - 11470
反应条件
tris-(dibenzylideneacetone)dipalladium(0) in 1,4-dioxane
反应条件
ethanol; hydrazine hydrate Behandeln des Reaktionsgemisches mit wss.Salzsaeure;
参考文献
Vermeulen, Martijn; Zwanenburg, Binne; Chittenden, Gordon J.F.; Verhagen, Hans
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 7-8 p. 729 - 737
反应条件
bis(benzonitrile)palladium(II) dichloride; AgNO2; CuCl2·2H2O; nitromethane; oxygen; tert-butyl alcohol T=20°C; Wacker Oxidation; P=760.051 Torr; 6 h;
参考文献
Wickens, Zachary K.; Morandi, Bill; Grubbs, Robert H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 43 p. 11257 - 11260
Angew. Chem., 2013 , vol. 125, # 43 p. 11467 - 11470
反应条件
hydrazine hydrate in ethanol 1 h;
参考文献
McNaughton, Brian R.; Bucholtz, Kevin M.; Camaano-Moure, Ana; Miller, Benjamin L.
Organic Letters, 2005 , vol. 7, # 4 p. 733 - 736
反应条件
dimethylsulfide; sodium acetate; ozone 1) MeOH, CH2Cl2, -78 deg C;; Yield given. Multistep reaction;
参考文献
Jiranusornkul, Supat; Sirithunyalug, Busaban; Nemoto, Hideo; Takahata, Hiroki
Heterocycles, 2002 , vol. 56, # 1-2 p. 487 - 496
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform
T=20°C; 18 h;
参考文献
Incarvito; Lam; Rhatigan; Rheingold; Jin Qin; Gavrilova; Bosnich
Journal of the Chemical Society, Dalton Transactions, 2001 , # 23 p. 3478 - 3488
