N-(4-烯丁基)邻苯二甲酰亚胺合成路线 （共 22 条）
反应条件
in dichloromethane
T=0 - 20°C; 48 h;
参考文献
Klinge Pharma GmbH
Patent: US6903118 B1, 2005 ;
Location in patent: Page/Page column 162-163 ;
反应条件
1: 79 percent / 3-chloroperoxybenzoic acid, 3-tert-butyl-4-hydroxy-5-methylphenyl sulphide / 1,2-dichloro-ethane / 1.) RT, 18 h, 2.) reflux, 1h
2: 64 percent / K2CO3 / ethanol / 6 h / Heating
View Scheme
参考文献
Ahmed; Stratford; Jenkins
Arzneimittel-Forschung/Drug Research, 1985 , vol. 35, # 12 p. 1763 - 1768
