N-甲氧基-N-甲基-4-硝基苯甲酰胺合成路线 （共 9 条）
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78 - -40°C; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; hexane; water T=0 - 20°C; Inert atmosphere;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
Schwartz's reagent in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Spletstoser, Jared T.; White, Jonathan M.; Tunoori, Ashok Rao; Georg, Gunda I.
Journal of the American Chemical Society, 2007 , vol. 129, # 11 p. 3408 - 3419
参考文献
Persson, Tobias; Nielsen, John
Organic Letters, 2006 , vol. 8, # 15 p. 3219 - 3222
反应条件
triethylamine in dichloromethane
T=0 - 18°C; 16.5 h; Inert atmosphere;
参考文献
Muir, Calum W.; Kennedy, Alan R.; Redmond, Joanna M.; Watson, Allan J. B.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 20 p. 3337 - 3340
反应条件
1: 4-nitro-benzoic acid With triethylamine; trichloromethyl chloroformate in dichloromethane
T=0°C;
2: O,N-dimethyl-hydroxylamine hydrochloride in dichloromethane
T=25°C; 1 h;
参考文献
Kim, Misoo; Lee, Hagyoung; Han, Ki-Jong; Kay, Kwang-Yol
Synthetic Communications, 2003 , vol. 33, # 23 p. 4013 - 4018
反应条件
1: 4-methoxy-benzoic acid With diethyl chlorophosphate in pyridine
T=20°C; Inert atmosphere;
2: O,N-dimethyl-hydroxylamine hydrochloride in pyridine
T=70°C; Inert atmosphere;
参考文献
McNulty, James; Krishnamoorthy, Venkatesan; Robertson, Al
Tetrahedron Letters, 2008 , vol. 49, # 44 p. 6344 - 6347
反应条件
in methanol
T=30°C; 3 h;
参考文献
Fountain; Felkerson, Cassie J.; Driskell, Jeremy D.; Lamp, Brian D.
Journal of Organic Chemistry, 2003 , vol. 68, # 5 p. 1810 - 1814
反应条件
in methanol-d4
T=30°C; correlation of reaction electron demands with α-effect for methyl transfer observed; Rate constant;
参考文献
Fountain; Dunkin, Timothy W.; Patel, Kamlesh D.
Journal of Organic Chemistry, 1997 , vol. 62, # 9 p. 2738 - 2741
反应条件
in methanol-d4
T=29.5°C; Rate constant;
参考文献
Fountain, Kenneth R.; Fountain, Daniel P.; Michaels, Bernice; Myers, D. Brenton; Salmon, Jon K.; et al.
Canadian Journal of Chemistry, 1991 , vol. 69, # 5 p. 798 - 810
