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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘苯甲醚
合成路线
（共 385 条）
529-28-2
2-碘苯甲醚
+
498-66-8
降冰片烯
→
反应条件
24423-09-4
反应条件
1-methyl-pyrrolidin-2-one; potassium carbonate; benzyl alcohol; palladium diacetate T=105°C; 24 h;
参考文献
Deledda, Sara; Motti, Elena; Catellani, Marta
Canadian Journal of Chemistry, 2005 , vol. 83, # 6-7 p. 741 - 747
766-85-8
3-碘苯甲醚
+
529-28-2
2-碘苯甲醚
→
反应条件
24423-09-4
反应条件
暂无反应条件数据
参考文献
Abramovitch,R.A.; Koleoso,O.A.
Journal of the Chemical Society [Section] B: Physical Organic, 1969 , vol. <B>, p. 779 - 785
529-28-2
2-碘苯甲醚
+
536-74-3
苯乙炔
→
反应条件
246230-86-4
3-碘-2-苯基-苯并呋喃
反应条件
1: phenylacetylene With n-butyllithium; boric acid trimethyl ester in ethylene glycol dimethyl ether; hexane T=-78 - 20°C; 1.75 h; 2: 1-iodo-2-methoxybenzene With triphenylphosphine; palladium diacetate in ethylene glycol dimethyl ether 4 h; Heating; 3: With N-iodo-succinimide; boron trichloride in hexane; dichloromethane T=20°C;
参考文献
Colobert, Francoise; Castanet, Anne-Sophie; Abillard, Olivier
European Journal of Organic Chemistry, 2005 , # 15 p. 3334 - 3341
273-53-0
苯并恶唑
+
529-28-2
2-碘苯甲醚
→
反应条件
13459-17-1
反应条件
potassium carbonate; copper(II) oxide in diethylene glycol dimethyl ether 3 h; Inert atmosphereReflux;
参考文献
Zhang, Wu; Zeng, Qinglong; Zhang, Xinming; Tian, Yujie; Yue, Yun; Guo, Yujun; Wang, Zhenghua
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4741 - 4745
529-28-2
2-碘苯甲醚
+
108-95-2
苯酚
→
反应条件
1695-04-1
2-甲氧基苯基苯醚
反应条件
pyridine-2-carboxylic acid; potassium phosphate; copper(l) iodide in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Maiti, Debabrata; Buchwald, Stephen L.
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1791 - 1794
529-28-2
2-碘苯甲醚
+
931-50-0
环己基溴化镁
→
反应条件
2206-48-6
1-环己基-2-甲氧基苯
反应条件
1: cyclohexyl magnesium bromide With zinc(II) chloride in tetrahydrofuran T=20°C; 1 h; 2: 1-iodo-2-methoxybenzene With dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran T=20°C; Negishi coupling; 2 h; Further stages.;
参考文献
Luo, Xiancai; Zhang, Heng; Duan, Hui; Liu, Qiang; Zhu, Lizheng; Zhang, Tony; Lei, Aiwen
Organic Letters, 2007 , vol. 9, # 22 p. 4571 - 4574
→
反应条件
21209-78-9
反应条件
PdCl2(dppf) (1 molpercent) in acetonitrile byproducts: C6H4(OCH3)C2(C6H5); 24 h;
参考文献
Hashmi, A. Stephen K.; Lothschuetz, Christian; Doepp, Rene; Rudolph, Matthias; Ramamurthi, Tanuja D.; Rominger, Frank
Angewandte Chemie - International Edition, 2009 , vol. 48, # 44 p. 8243 - 8246
127591-24-6
+
529-28-2
2-碘苯甲醚
→
反应条件
21209-78-9
反应条件
PdCl2(dppf) (1 molpercent) in acetonitrile byproducts: (CH3O)C6H4C6H4OCH3; 48 h;
参考文献
Hashmi, A. Stephen K.; Lothschuetz, Christian; Doepp, Rene; Rudolph, Matthias; Ramamurthi, Tanuja D.; Rominger, Frank
Angewandte Chemie - International Edition, 2009 , vol. 48, # 44 p. 8243 - 8246
37766-89-5
+
529-28-2
2-碘苯甲醚
→
反应条件
21209-78-9
反应条件
PdCl2(dppf) (1 molpercent) in acetonitrile byproducts: C6H4(OCH3)(CHCH2); 24 h;
参考文献
Hashmi, A. Stephen K.; Lothschuetz, Christian; Doepp, Rene; Rudolph, Matthias; Ramamurthi, Tanuja D.; Rominger, Frank
Angewandte Chemie - International Edition, 2009 , vol. 48, # 44 p. 8243 - 8246
529-28-2
2-碘苯甲醚
→
反应条件
28748-41-6
反应条件
1: 66 percent / tBuOK / liquid ammonia / -33 °C / Irradiation 2: 1) ClSiMe3, NaI View Scheme
参考文献
Beugelmans, Rene; Ginsburg, Helene
Journal of the Chemical Society, Chemical Communications, 1980 , # 11 p. 508 - 509
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