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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-碘苯甲醚
合成路线
（共 385 条）
529-28-2
2-碘苯甲醚
+
90-04-0
邻甲氧基苯胺
→
反应条件
7287-74-3
反应条件
18-crown-6 ether; copper; potassium carbonate in 1,2-dichloro-benzene 48 h; Heating;
参考文献
Bushby, Richard J.; McGill, David R.; Ng, Kai M.; Taylor, Norman
Journal of Materials Chemistry, 1997 , vol. 7, # 12 p. 2343 - 2354
529-28-2
2-碘苯甲醚
→
反应条件
7288-07-5
反应条件
1: 91 percent / K2CO3, Cu, 18-crown-6 / 1,2-dichloro-benzene / 48 h / Heating 2: 97 percent / BBr3 / CH2Cl2 / -78 - 20 °C View Scheme
参考文献
Frye,C.L. et al.
Journal of the American Chemical Society, 1966 , vol. 88, p. 2727 - 2730
529-28-2
2-碘苯甲醚
+
68-12-2
N,N-二甲基甲酰胺
→
反应条件
7291-34-1
2-甲氧基-N,N-二甲基-苯甲酰胺
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate T=135°C; 6 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5489 - 5494
529-28-2
2-碘苯甲醚
+
53915-69-8
1,2-丙二烯三正丁基锡
→
反应条件
73234-94-3
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in N,N-dimethyl-formamide T=50°C; 24 h;
参考文献
Huang, Chih-Wei; Shanmugasundaram, Muthian; Chang, Hao-Ming; Cheng, Chien-Hong
Tetrahedron, 2003 , vol. 59, # 20 p. 3635 - 3641
→
反应条件
73234-94-3
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium methylate in N,N-dimethyl-formamide T=20°C; Suzuki-Miyaura cross coupling reaction; 3 h; Inert atmosphere;
参考文献
Radkowski, Karin; Seidel, Guenter; Fuerstner, Alois
Chemistry Letters, 2011 , vol. 40, # 9 p. 950 - 952
529-28-2
2-碘苯甲醚
→
反应条件
73234-94-3
+
66021-98-5
反应条件
1: triethylamine; tetrakis(triphenylphosphine) palladium(0); copper(l) iodide / tetrahydrofuran / 12 h / 40 °C 2: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 3 h / 0 °C / |Darkness 3: diethylzinc; oxygen / dichloromethane; n-heptane / 14 h / 20 °C / |Darkness View Scheme
参考文献
Jammi, Suribabu; Mouysset, Dominique; Siri, Didier; Bertrand, Michele P.; Feray, Laurence
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1589 - 1603
529-28-2
2-碘苯甲醚
+
471-25-0
→
反应条件
7342-00-9
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane in dimethyl sulfoxide T=50°C; Sonogashira coupling; 5 h; Sealed flask;
参考文献
Park, Kyungho; Palani, Thiruvengadam; Pyo, Ayoung; Lee, Sunwoo
Tetrahedron Letters, 2012 , vol. 53, # 7 p. 733 - 737
529-28-2
2-碘苯甲醚
→
反应条件
7342-00-9
反应条件
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C 1.2: 9 h / -78 - 20 °C 1.3: 50 °C / Inert atmosphere 2.1: water; potassium hydroxide / methanol / 12 h / 25 °C View Scheme
参考文献
Hapke, Marko; Kral, Karolin; Spannenberg, Anke
Synthesis, 2011 , # 4 art. no. Z27710SS, p. 642 - 652
529-28-2
2-碘苯甲醚
→
反应条件
74129-03-6
反应条件
1: 25 percent / copper / 6 h / 220 - 240 °C 2: 76 percent / hydrobromic acid, acetic acid / 18 h / Heating 3: 26 percent / acetic acid, water, sodium nitrite / 5 °C 4: 97 percent / 1 N sodium carbonate, sodium dithionite / 5 h / 35 °C 5: methanol 6: 84 percent / ethanol; H2O / Heating 7: 6 N aq. HCl / Heating 8: ethanol / Heating View Scheme
参考文献
Werbel; Cook; Elslager; Hung; Johnson; Kesten; McNamara; Ortwine; Worth
Journal of Medicinal Chemistry, 1986 , vol. 29, # 6 p. 924 - 939
529-28-2
2-碘苯甲醚
→
反应条件
7451-95-8
反应条件
1: 40 percent / tBuOK / liquid ammonia / -33 °C / Irradiation 2: ClSiMe3, NaI View Scheme
参考文献
Beugelmans, Rene; Ginsburg, Helene
Journal of the Chemical Society, Chemical Communications, 1980 , # 11 p. 508 - 509
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