1,2,3,4-四氢-1-萘酚合成路线 (共 211 条)
反应条件
lipase from Pseudomonas cepacia immobilized on ceramic in toluene T=40°C; 4 h;
参考文献
Ghanem, Ashraf; Schurig, Volker
Monatshefte fur Chemie, 2003 , vol. 134, # 8 p. 1151 - 1157
反应条件
Pseudomonas cepacia lipase; 4 A molecular sieve; peracetylated-β-cyclodextrin in toluene T=40°C; 2 h; Title compound not separated from byproducts;
参考文献
Ghanem, Ashraf; Schurig, Volker
Tetrahedron Asymmetry, 2003 , vol. 14, # 17 p. 2547 - 2555
反应条件
2-acetyloxy-1-propene; lipase YS in di-isopropyl ether T=30°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Naemura, Koichiro; Fukuda, Ritsuko; Konishi, Masayoshi; Hirose, Keiji; Tobe, Yoshito
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 10 p. 1253 - 1256
反应条件
(-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=-78°C; 20 h; Inert atmosphereMolecular sieve; optical yield given as percent ee;
参考文献
Klauck, Maggie I.; Patel, Sachin G.; Wiskur, Sheryl L.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3570 - 3575
反应条件
lipase YS in di-isopropyl ether T=30°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Naemura, Koichiro; Fukuda, Ritsuko; Konishi, Masayoshi; Hirose, Keiji; Tobe, Yoshito
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 10 p. 1253 - 1256
反应条件
(-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=-78°C; 20 h; Inert atmosphereMolecular sieve; optical yield given as percent ee;
参考文献
Klauck, Maggie I.; Patel, Sachin G.; Wiskur, Sheryl L.
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3570 - 3575
反应条件
lipase Amano PS30 in various solvent(s) Enzymatic reaction;
参考文献
Merlic; Walsh
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2265 - 2274
反应条件
in hexane Acylation; isobutylation; 18 h; Heating; Title compound not separated from byproducts;
参考文献
Yamada, Shinji; Katsumata, Hiroko
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9365 - 9373
反应条件
in benzene T=35°C; 2.5 h; Irradiationporcine pancreas lipase-catalyzed; microwave irradiation; ee investigated; Rate constantProduct distribution;
参考文献
Lin, Gialih; Lin, Wen-Yuan
Tetrahedron Letters, 1998 , vol. 39, # 24 p. 4333 - 4336
反应条件
in benzene 2.5 h; HeatingIrradiationporcine pancreas lipase-catalyzed; microwave irradiation; ee investigated; Rate constantProduct distribution;
参考文献
Lin, Gialih; Lin, Wen-Yuan
Tetrahedron Letters, 1998 , vol. 39, # 24 p. 4333 - 4336