1,2,3,4-四氢-1-萘酚合成路线 （共 211 条）
反应条件
1: 98 percent / thionyl chloride / toluene / 20 - 55 °C / microwave irradiation 2: 90 percent / potassium carbonate; sodium iodide / dimethylformamide / 1.17 h / 80 - 120 °C / microwave irradiation 3: 95 percent / KOH / H2O; methanol / 1 h / 70 - 90 °C / microwave irradiation View Scheme
参考文献
El-Ahmad, Youssef; Maillet, Philippe; Laurent, Elisabeth; Talab, Akram; Tran, Gilles; Ollivier, Roland
Heterocycles, 1997 , vol. 45, # 4 p. 723 - 734
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran T=0°C; Mitsunobu reaction; 16 h;
参考文献
NOVARTIS AG
Patent: WO2008/76336 A2, 2008 ;
Location in patent: Page/Page column 65-66 ;
WO 2008/076336 A2
反应条件
1: p-toluenesulfonic acid monohydrate / benzene / 0.5 h / Heating 2: m-chloroperbenzoic acid / CH2Cl2 / 12 h / 0 °C 3: p-toluenesulfonic acid monohydrate / toluene / 1.5 h / Heating View Scheme
参考文献
Vebrel, Joel; Carrie, Robert
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 5-6 p. 161 - 166
反应条件
T=600 - 650°C; Leiten ueber einen CaO-Fe2O3-Katalysator;
参考文献
Koppers Co.
Patent: US2595266 , 1948 ;
反应条件
copper(II) sulfate in neat (no solvent) T=140°C; P=25 Torr; 0.5 h;
参考文献
Neudeck, Horst; Brinker, Udo H.
Tetrahedron Letters, 2005 , vol. 46, # 11 p. 1893 - 1895
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane T=20°C; 24 h;
参考文献
Noji, Masahiro; Ohno, Tomoko; Fuji, Koji; Futaba, Noriko; Tajima, Hiroyuki; Ishii, Keitaro
Journal of Organic Chemistry, 2003 , vol. 68, # 24 p. 9340 - 9347
反应条件
tetrachlorosilane in chloroform T=20°C; 5 h;
参考文献
Firouzabadi, Habib; Iranpoor, Naser; Karimi, Babak; Hazarkhani, Hassan
Synthetic Communications, 2003 , vol. 33, # 21 p. 3671 - 3677
反应条件
toluene-4-sulfonic acid in dichloromethane Heating;
参考文献
Sanz, Roberto; Martinez, Alberto; Miguel, Delia; Alvarez-Gutierrez, Julia M.; Rodriguez, Felix
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 14 p. 1841 - 1845
反应条件
silica gel supported sodium hydrogen sulfate in 1,2-dichloro-ethane T=30°C; 0.5 h;
参考文献
Sato, Yuta; Aoyama, Tadashi; Takido, Toshio; Kodomari, Mitsuo
Tetrahedron, 2012 , vol. 68, # 35 p. 7077 - 7081
反应条件
FeCl3·6H2O in 1,2-dichloro-ethane T=100°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Li, Wenjuan; Zheng, Xiaojian; Li, Zhiping
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 181 - 190
