1,2,3,4-四氢-1-萘酚合成路线 (共 211 条)
反应条件
n-butyllithium in hexane
反应条件
N-(quinolin-2-ylmethylidene)aniline; copper(II) bis(trifluoromethanesulfonate); phenylhydrazine in acetone T=30°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Tetrahedron, , vol. 69, # 8 p. 2033 - 2037
反应条件
N-(quinolin-2-ylmethylidene)aniline; copper(II) bis(trifluoromethanesulfonate); phenylhydrazine in acetone T=30°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Tetrahedron, , vol. 69, # 8 p. 2033 - 2037
反应条件
N-(quinolin-2-ylmethylidene)aniline; copper(II) bis(trifluoromethanesulfonate); phenylhydrazine in acetone T=30°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Tetrahedron, , vol. 69, # 8 p. 2033 - 2037
反应条件
tetrabutylammomium bromide; copper dichloride in dichloromethane T=25°C; 4 h; Further byproducts given;
参考文献
Feldberg, Liron; Sasson, Yoel
Tetrahedron Letters, 1996 , vol. 37, # 12 p. 2063 - 2066
反应条件
Oxonereg; in methanol 0.15 h; Heating;
参考文献
Mohammadpoor-Baltork; Amini; Farshidipoor
Bulletin of the Chemical Society of Japan, 2000 , vol. 73, # 12 p. 2775 - 2778
反应条件
hydrogen; palladium on activated charcoal in various solvent(s) T=109.85°C; P=3750.3 Torr; 1 h;
参考文献
Chemistry Letters, , vol. 35, # 7 p. 780 - 781
反应条件
tert.-butylhydroperoxide; C45H52CuN4O3 in decane; acetonitrile T=70°C; 36 h; Reflux;
参考文献
European Journal of Organic Chemistry, , # 4 p. 503 - 509
反应条件
1: iso-propylmagnesium bromide With trimethylsilyl-methylmagnesium chloride; lithium chloride; zinc(II) chloride in tetrahydrofuran; diethyl ether T=20°C; 0.75 h; Inert atmosphere; 2: 3,4-dihydronaphthalene-1(2H)-one in tetrahydrofuran; diethyl ether T=0°C; 3 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 15 p. 5008 - 5016
反应条件
1: ethylmagnesium bromide With zinc(II) chloride in tetrahydrofuran T=20°C; 0.75 h; Inert atmosphere; 2: 3,4-dihydronaphthalene-1(2H)-one in tetrahydrofuran T=0°C; 3 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 15 p. 5008 - 5016